Synthesis of NiO nanoparticles via thermolysis of (phenanthroline)NiCl2 complex
| dc.contributor.author | Barakat, Assem | |
| dc.date.accessioned | 2018-01-24T12:54:08Z | |
| dc.date.available | 2018-01-24T12:54:08Z | |
| dc.date.issued | 2016-03-23 | |
| dc.description.abstract | The synthesized (2,9-dimethyl-1,10-phenanthroline)NiClR2R complex (see the Scheme) was characterized by elemental analysis, IR spectroscopy, UV-vis spectroscopy and differential thermal/thermogravimetric analysis (TG/DTA). The 3D structure of the desired complex was solved by single crystal X-ray diffraction (XRD) as triclinic system. The desired complex, subjected to thermal decomposition at low temperature of 400 °C in an open atmosphere, revealed a novel and facile synthesis of pure NiO nanoparticles with uniform spherical particle; the structure of the NiO nanoparticles product was elucidated on the basis of Fourier transform infrared (FT-IR), UV-vis spectroscopy, TG/DTA, XRD, scanning electron microscopy (SEM), energy-dispersive X-ray spectrometry (EDXS) and transmission electron microscopy (TEM). | en_US |
| dc.identifier.uri | https://hdl.handle.net/20.500.11888/13060 | |
| dc.language.iso | en | en_US |
| dc.title | Synthesis of NiO nanoparticles via thermolysis of (phenanthroline)NiCl2 complex | en_US |
| dc.type | Article | en_US |
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