Synthesis and characterization of metal oxide nanoparticles (MON): cases of MgO and FeO

Prepared by:
Hala Odeh 
Safia Kahla
Shiraz Hussein 
 
Supervisor:
Dr.Hamdallah Bearat 



Objectives 
Overview 
Introduction 
Synthesis and characterization 
Results and discussion
Errors and difficulties 
Conclusion 
Recommendations



Overview
The first stage  of  research concerns about synthesis of two metal oxides: (I) magnesium oxide (MgO) through thermal methods starting from the carbonate (MgCO3) , (ii) ferric iron oxide (Fe­2O3) through thermal or hydrothermal decomposition of iron oxyhydroxid (FeO.OH).
While in the second stage,  the product is analyzed as powders for particle size and particle size distribution using  the following technique: X-ray powder diffraction (XRD).



Introduction
The project  focus on  synthesis and characterization of MgO and FeO
Where the Characterization part include checking and testing the samples available by different devices like XRD , SEM , TEM , UV and etc . But the device that was chosen to check the size of the samples is XRD , as it’s the only device available in our country specifically in Arab American University – Jenin .



What is X-Ray Diffraction?
 X-ray powder diffraction (XRD) is a rapid analytical technique used for phase identification of a crystalline material ,provide information on unit cell dimensions, and for determining the mean size of Nano crystallites. Both phases of MgO & Feo demonstrates very sharp peak . As shown later in results 


Synthesis OF MgO and FeO
Preparation of MgO
Dry Magnesium carbonate in oven at 90C ⸰
    MgCO3∆→MgO+CO2
Weigh a sample of 1g MgO 
Heat it at different temperature using electric furnace 

Preparation of FeO
Dry iron oxide  in oven at 90C ⸰
     2FeO.OH∆→Fe2O3 + H2O
Weigh a sample of 0.5g Fe₂O ₃
Heat it at different temperature using electric furnace 



Characterization 
XRD TEST:
Different samples were chosen to apply them for the test, the steps were:
Preparation of powder samples 
Put the sample on the specified glass for the device.
Insert the sample inside the device for the test by closing on it.
Insert the wanted data like speed, range of angle and etc on the software.
The Miniflex program starts drawing the graph of  2θ versus intensity. 


Results and Discussion 
The best samples were taken to test them in the XRD. As mentioned earlier that the range of diameter of a Nano particle is from (0-100) nm, and the diameter of the samples didn’t exceed 50nm .When the temperature increase the size of the diameter increase, it was noticed also that as the temperature rise the width of the peak get narrower.






                     

	Sample temp. ©	Diameter(nano meter)
	600	2.602733
 
	700	2.954923
 
	800	3.751513
 

Table (1):MgO temperature series at 10min and 2deg per min



Figure(1):MgO temperature series @10min and 2deg per min


temp.series for Mgo

MgO 10 min 600 C 2 deg per min	20	20.05	20.100000000000001	20.149999999999999	20.2	20.25	20.3	20.350000000000001	20.399999999999999	20.45	20.5	20.55	20.6	20.65	20.7	20.75	20.8	20.85	20.9	20.95	21	21.05	21.1	21.15	21.2	21.25	21.3	21.35	21.4	21.45	21.5	21.55	21.6	21.65	21.7	21.75	21.8	21.85	21.9	21.95	22	22.05	22.1	22.15	22.2	22.25	22.3	22.35	22.4	22.45	22.5	22.55	22.6	22.65	22.7	22.75	22.8	22.85	22.9	22.95	23	23.05	23.1	23.15	23.2	23.25	23.3	23.35	23.4	23.45	23.5	23.55	23.6	23.65	23.7	23.75	23.8	23.85	23.9	23.95	24	24.05	24.1	24.15	24.2	24.25	24.3	24.35	24.4	24.45	24.5	24.55	24.6	24.6	5	24.7	24.75	24.8	24.85	24.9	24.95	25	25.05	25.1	25.15	25.2	25.25	25.3	25.35	25.4	25.45	25.5	25.55	25.6	25.65	25.7	25.75	25.8	25.85	25.9	25.95	26	26.05	26.1	26.15	26.2	26.25	26.3	26.35	26.4	26.45	26.5	26.55	26.6	26.65	26.7	26.75	26.8	26.85	26.9	26.95	27	27.05	27.1	27.15	27.2	27.25	27.3	27.35	27.4	27.45	27.5	27.55	27.6	27.65	27.7	27.75	27.8	27.85	27.9	27.95	28	28.05	28.1	28.15	28.2	28.25	28.3	28.35	28.4	28.45	28.5	28.55	28.6	28.65	28.7	28.75	28.8	28.85	28.9	28.95	29	29.05	29.1	29.15	29.2	29.25	29.3	29.35	29.4	29.45	29.5	29.55	29.6	29.65	29.7	29.75	29.8	29.85	29.9	29.95	30	30.05	30.1	30.15	30.2	30.25	30.3	30.35	30.4	30.45	30.5	30.55	30.6	30.65	30.7	30.75	30.8	30.85	30.9	30.95	31	31.05	31.1	31.15	31.2	31.25	31.3	31.35	31.4	31.45	31.5	31.55	31.6	31.65	31.7	31.75	31.8	31.85	31.9	31.95	32	32.049999999999997	32.1	32.15	32.200000000000003	32.25	32.299999999999997	32.35	32.4	32.450000000000003	32.5	32.549999999999997	32.6	32.65	32.700000000000003	32.75	32.799999999999997	32.85	32.9	32.950000000000003	33	33.049999999999997	33.1	33.15	33.200000000000003	33.25	33.299999999999997	33.35	33.4	33.450000000000003	33.5	33.549999999999997	33.6	33.65	33.700000000000003	33.75	33.799999999999997	33.85	33.9	33.950000000000003	34	34.049999999999997	34.1	34.15	34.200000000000003	34.25	34.299999999999997	34.35	34.4	34.450000000000003	34.5	34.549999999999997	34.6	34.65	34.700000000000003	34.75	34.799999999999997	34.85	34.9	34.950000000000003	35	35.049999999999997	35.1	35.15	35.200000000000003	35.25	35.299999999999997	35.35	35.4	35.450000000000003	35.5	35.549999999999997	35.6	35.65	35.700000000000003	35.75	35.799999999999997	35.85	35.9	35.950000000000003	36	36.049999999999997	36.1	36.15	36.200000000000003	36.25	36.299999999999997	36.35	36.4	36.450000000000003	36.5	36.549999999999997	36.6	36.65	36.700000000000003	36.75	36.799999999999997	36.85	36.9	36.950000000000003	37	37.049999999999997	37.1	37.15	37.200000000000003	37.25	37.299999999999997	37.35	37.4	37.450000000000003	37.5	37.549999999999997	37.6	37.65	37.700000000000003	37.75	37.799999999999997	37.85	37.9	37.950000000000003	38	38.049999999999997	38.1	38.15	38.200000000000003	38.25	38.299999999999997	38.35	38.4	38.450000000000003	38.5	38.549999999999997	38.6	38.65	38.700000000000003	38.75	38.799999999999997	38.85	38.9	38.950000000000003	39	39.049999999999997	39.1	39.15	39.200000000000003	39.25	39.299999999999997	39.35	39.4	39.450000000000003	39.5	39.549999999999997	39.6	39.65	39.700000000000003	39.75	39.799999999999997	39.85	39.9	39.950000000000003	40	40.049999999999997	40.1	40.15	40.200000000000003	40.25	40.299999999999997	40.35	40.4	40.450000000000003	40.5	40.549999999999997	40.6	40.65	40.700000000000003	40.75	40.799999999999997	40.85	40.9	40.950000000000003	41	41.05	41.1	41.15	41.2	41.25	41.3	41.35	41.4	41.45	41.5	41.55	41.6	41.65	41.7	41.75	41.8	41.85	41.9	41.95	42	42.05	42.1	42.15	42.2	42.25	42.3	42.35	42.4	42.45	42.5	42.55	42.6	42.65	42.7	42.75	42.8	42.85	42.9	42.95	43	43.05	43.1	43.15	43.2	43.25	43.3	43.35	43.4	43.45	43.5	43.55	43.6	43.65	43.7	43.75	43.8	43.85	43.9	43.95	44	44.05	44.1	44.15	44.2	44.25	44.3	44.35	44.4	44.45	44.5	44.55	44.6	44.65	44.7	44.75	44.8	44.85	44.9	44.95	45	45.05	45.1	45.15	45.2	45.25	45.3	45.35	45.4	45.45	45.5	45.55	45.6	45.65	45.7	45.75	45.8	45.85	45.9	45.95	46	46.05	46.1	46.15	46.2	46.25	46.3	46.35	46.4	46.45	46.5	46.55	46.6	46.65	46.7	46.75	46.8	46.85	46.9	46.95	47	47.05	47.1	47.15	47.2	47.25	47.3	47.35	47.4	47.45	47.5	47.55	47.6	47.65	47.7	47.75	47.8	47.85	47.9	47.95	48	48.05	48.1	48.15	48.2	48.25	48.3	48.35	48.4	48.45	48.5	48.55	48.6	48.65	48.7	48.75	48.8	48.85	48.9	48.95	49	49.05	49.1	49.15	49.2	49.25	49.3	49.35	49.4	49.45	49.5	49.55	49.6	49.65	49.7	49.75	49.8	49.85	49.9	49.95	50	50.05	50.1	50.15	50.2	50.25	50.3	50.35	50.4	50.45	50.5	50.55	50.6	50.65	50.7	50.75	50.8	50.85	50.9	50.95	51	51.05	51.1	51.15	51.2	51.25	51.3	51.35	51.4	51.45	51.5	51.55	51.6	51.65	51.7	51.75	51.8	51.85	51.9	51.95	52	52.05	52.1	52.15	52.2	52.25	52.3	52.35	52.4	52.45	52.5	52.55	52.6	52.65	52.7	52.75	52.8	52.85	52.9	52.95	53	53.05	53.1	53.15	53.2	53.25	53.3	53.35	53.4	53.45	53.5	53.55	53.6	53.65	53.7	53.75	53.8	53.85	53.9	53.95	54	54.05	54.1	54.15	54.2	54.25	54.3	54.35	54.4	54.45	54.5	54.55	54.6	54.65	54.7	54.75	54.8	54.85	54.9	54.95	55	55.05	55.1	55.15	55.2	55.25	55.3	55.35	55.4	55.45	55.5	55.55	55.6	55.65	55.7	55.75	55.8	55.85	55.9	55.95	56	56.05	56.1	56.15	56.2	56.25	56.3	56.35	56.4	56.45	56.5	56.55	56.6	56.65	56.7	56.75	56.8	56.85	56.9	56.95	57	57.05	57.1	57.15	57.2	57.25	57.3	57.35	57.4	57.45	57.5	57.55	57.6	57.65	57.7	57.75	57.8	57.85	57.9	57.95	58	58.05	58.1	58.15	58.2	58.25	58.3	58.35	58.4	58.45	58.5	58.55	58.6	58.65	58.7	58.75	58.8	58.85	58.9	58.95	59	59.05	59.1	59.15	59.2	59.25	59.3	59.35	59.4	59.45	59.5	59.55	59.6	59.65	59.7	59.75	59.8	59.85	59.9	59.95	60	117	112	108	106	127	108	99	111	112	115	101	100	139	110	134	115	105	101	104	104	120	119	109	102	93	110	114	96	120	92	114	108	113	110	114	104	93	98	99	109	112	111	97	122	113	93	97	93	102	129	95	110	106	117	125	119	97	121	137	120	111	114	133	121	118	151	119	134	106	130	142	119	123	122	138	115	122	120	116	123	124	100	110	109	103	99	117	112	122	125	103	118	116	101	113	113	96	123	111	122	106	104	107	104	115	126	115	115	108	108	111	99	99	100	110	109	103	113	100	130	105	99	131	126	107	122	114	107	103	109	102	123	101	126	102	126	100	96	104	97	96	112	108	120	125	112	122	120	113	119	106	108	111	109	132	111	120	104	107	120	87	93	130	114	104	119	100	108	101	120	91	100	109	95	107	120	115	123	119	124	103	121	121	123	108	107	126	108	104	112	102	138	109	112	108	130	138	122	126	112	143	152	141	143	158	170	131	125	135	135	105	115	133	110	105	102	123	114	134	121	103	104	109	100	102	115	130	115	98	93	118	88	122	107	108	113	98	122	101	120	121	117	93	119	119	125	109	118	113	102	125	109	93	106	100	129	110	135	92	127	117	101	96	98	104	112	121	124	133	126	126	122	101	109	119	100	116	113	108	115	121	119	129	109	106	128	127	115	114	123	126	131	115	133	112	124	118	110	127	129	119	110	125	122	127	125	127	119	135	118	96	111	113	106	110	136	150	138	132	118	119	107	126	153	125	130	117	111	119	118	131	133	132	126	132	140	139	157	158	147	128	142	135	129	129	147	148	151	125	140	141	155	163	155	148	143	154	168	122	153	174	139	166	178	174	170	170	180	173	166	168	168	190	171	203	189	207	201	198	193	197	190	199	173	187	182	208	176	212	186	168	186	140	168	166	165	150	145	143	158	138	137	158	153	147	145	136	132	130	154	158	137	125	109	127	117	130	114	139	109	113	144	165	120	121	125	117	118	147	133	143	134	122	126	117	139	122	139	143	132	163	154	160	159	134	205	175	184	178	168	210	195	235	197	225	263	260	276	272	282	311	342	336	336	328	371	370	359	377	370	394	382	354	358	356	353	341	338	295	273	278	291	256	222	221	207	205	208	196	157	163	120	183	161	158	157	150	108	134	123	121	144	129	120	117	144	144	120	125	115	92	129	106	100	82	106	98	98	110	122	109	95	76	99	88	109	77	83	105	96	88	104	104	106	101	108	93	82	86	83	77	87	86	85	87	81	98	88	88	88	107	97	83	89	80	77	84	86	104	94	86	84	76	90	90	102	111	93	94	97	104	101	72	90	78	106	89	81	87	88	81	92	72	92	81	76	88	96	81	95	95	94	94	94	87	93	76	86	84	77	79	82	87	71	76	81	76	80	85	85	67	89	70	70	74	78	74	97	76	75	76	100	79	94	79	66	77	76	89	91	64	93	66	86	90	80	83	91	77	84	86	107	68	86	70	96	85	80	85	67	85	99	77	75	71	80	88	82	80	77	81	71	86	83	80	92	95	74	68	79	61	70	84	63	76	69	84	84	60	81	71	79	90	75	70	61	71	67	88	85	88	74	70	76	77	84	77	90	80	80	70	72	88	88	79	79	97	75	71	89	91	80	93	93	94	102	100	106	84	90	108	90	89	90	85	98	86	102	79	86	105	88	81	84	104	81	109	95	83	87	87	84	94	102	96	80	84	84	77	91	69	86	94	81	89	77	86	85	79	84	71	76	69	60	93	62	86	80	84	92	63	88	75	86	78	74	77	73	82	100	75	96	92	95	97	82	96	91	113	87	82	82	100	105	96	80	91	100	86	90	80	MgO 10 min700 C 2 deg per min	20	20.05	20.100000000000001	20.149999999999999	20.2	20.25	20.3	20.350000000000001	20.399999999999999	20.45	20.5	20.55	20.6	20.65	20.7	20.75	20.8	20.85	20.9	20.95	21	21.05	21.1	21.15	21.2	21.25	21.3	21.35	21.4	21.45	21.5	21.55	21.6	21.65	21.7	21.75	21.8	21.85	21.9	21.95	22	22.05	22.1	22.15	22.2	22.25	22.3	22.35	22.4	22.45	22.5	22.55	22.6	22.65	22.7	22.75	22.8	22.85	22.9	22.95	23	23.05	23.1	23.15	23.2	23.25	23.3	23.35	23.4	23.45	23.5	23.55	23.6	23.65	23.7	23.75	23.8	23.85	23.9	23.95	24	24.05	24.1	24.15	24.2	24.25	24.3	24.35	24.4	24.45	24.5	24.55	24.6	24.65	24.7	24.75	24.8	24.85	24.9	24.95	25	25.05	25.1	25.15	25.2	25.25	25.3	25.35	25.4	25.45	25.5	25.55	25.6	25.65	25.7	25.75	25.8	25.85	25.9	25.95	26	26.05	26.1	26.15	26.2	26.25	26.3	26.35	26.4	26.45	26.5	26.55	26.6	26.65	26	.7	26.75	26.8	26.85	26.9	26.95	27	27.05	27.1	27.15	27.2	27.25	27.3	27.35	27.4	27.45	27.5	27.55	27.6	27.65	27.7	27.75	27.8	27.85	27.9	27.95	28	28.05	28.1	28.15	28.2	28.25	28.3	28.35	28.4	28.45	28.5	28.55	28.6	28.65	28.7	28.75	28.8	28.85	28.9	28.95	29	29.05	29.1	29.15	29.2	29.25	29.3	29.35	29.4	29.45	29.5	29.55	29.6	29.65	29.7	29.75	29.8	29.85	29.9	29.95	30	30.05	30.1	30.15	30.2	30.25	30.3	30.35	30.4	30.45	30.5	30.55	30.6	30.65	30.7	30.75	30.8	30.85	30.9	30.95	31	31.05	31.1	31.15	31.2	31.25	31.3	31.35	31.4	31.45	31.5	31.55	31.6	31.65	31.7	31.75	31.8	31.85	31.9	31.95	32	32.049999999999997	32.1	32.15	32.200000000000003	32.25	32.299999999999997	32.35	32.4	32.450000000000003	32.5	32.549999999999997	32.6	32.65	32.700000000000003	32.75	32.799999999999997	32.85	32.9	32.950000000000003	33	33.049999999999997	33.1	33.15	33.200000000000003	33.25	33.299999999999997	33.35	33.4	33.450000000000003	33.5	33.549999999999997	33.6	33.65	33.700000000000003	33.75	33.799999999999997	33.85	33.9	33.950000000000003	34	34.049999999999997	34.1	34.15	34.200000000000003	34.25	34.299999999999997	34.35	34.4	34.450000000000003	34.5	34.549999999999997	34.6	34.65	34.700000000000003	34.75	34.799999999999997	34.85	34.9	34.950000000000003	35	35.049999999999997	35.1	35.15	35.200000000000003	35.25	35.299999999999997	35.35	35.4	35.450000000000003	35.5	35.549999999999997	35.6	35.65	35.700000000000003	35.75	35.799999999999997	35.85	35.9	35.950000000000003	36	36.049999999999997	36.1	36.15	36.200000000000003	36.25	36.299999999999997	36.35	36.4	36.450000000000003	36.5	36.549999999999997	36.6	36.65	36.7000	00000000003	36.75	36.799999999999997	36.85	36.9	36.950000000000003	37	37.049999999999997	37.1	37.15	37.200000000000003	37.25	37.299999999999997	37.35	37.4	37.450000000000003	37.5	37.549999999999997	37.6	37.65	37.700000000000003	37.75	37.799999999999997	37.85	37.9	37.950000000000003	38	38.049999999999997	38.1	38.15	38.200000000000003	38.25	38.299999999999997	38.35	38.4	38.450000000000003	38.5	38.549999999999997	38.6	38.65	38.700000000000003	38.75	38.799999999999997	38.85	38.9	38.950000000000003	39	39.049999999999997	39.1	39.15	39.200000000000003	39.25	39.299999999999997	39.35	39.4	39.450000000000003	39.5	39.549999999999997	39.6	39.65	39.700000000000003	39.75	39.799999999999997	39.85	39.9	39.950000000000003	40	40.049999999999997	40.1	40.15	40.200000000000003	40.25	40.299999999999997	40.35	40.4	40.450000000000003	40.5	40.549999999999997	40.6	40.65	40.700000000000003	40.75	40.799999999999997	40.85	40.9	40.950000000000003	41	41.05	41.1	41.15	41.2	41.25	41.3	41.35	41.4	41.45	41.5	41.55	41.6	41.65	41.7	41.75	41.8	41.85	41.9	41.95	42	42.05	42.1	42.15	42.2	42.25	42.3	42.35	42.4	42.45	42.5	42.55	42.6	42.65	42.7	42.75	42.8	42.85	42.9	42.95	43	43.05	43.1	43.15	43.2	43.25	43.3	43.35	43.4	43.45	43.5	43.55	43.6	43.65	43.7	43.75	43.8	43.85	43.9	43.95	44	44.05	44.1	44.15	44.2	44.25	44.3	44.35	44.4	44.45	44.5	44.55	44.6	44.65	44.7	44.75	44.8	44.85	44.9	44.95	45	45.05	45.1	45.15	45.2	45.25	45.3	45.35	45.4	45.45	45.5	45.55	45.6	45.65	45.7	45.75	45.8	45.85	45.9	45.95	46	46.05	46.1	46.15	46.2	46.25	46.3	46.35	46.4	46.45	46.5	46.55	46.6	46.65	46.7	46.75	46.8	46.85	46.9	46.95	47	47.05	47.1	47.15	47.2	47.25	47.3	47.35	47.4	47.45	47.5	47.55	47.6	47.65	47.7	47.75	47.8	47.85	47.9	47.95	48	48.05	48.1	48.15	48.2	48.25	48.3	48.35	48.4	48.45	48.5	48.55	48.6	48.65	48.7	48.75	48.8	48.85	48.9	48.95	49	49.05	49.1	49.15	49.2	49.25	49.3	49.35	49.4	49.45	49.5	49.55	49.6	49.65	49.7	49.75	49.8	49.85	49.9	49.95	50	50.05	50.1	50.15	50.2	50.25	50.3	50.35	50.4	50.45	50.5	50.55	50.6	50.65	50.7	50.75	50.8	50.85	50.9	50.95	51	51.05	51.1	51.15	51.2	51.25	51.3	51.35	51.4	51.45	51.5	51.55	51.6	51.65	51.7	51.75	51.8	51.85	51.9	51.95	52	52.05	52.1	52.15	52.2	52.25	52.3	52.35	52.4	52.45	52.5	52.55	52.6	52.65	52.7	52.75	52.8	52.85	52.9	52.95	53	53.05	53.1	53.15	53.2	53.25	53.3	53.35	53.4	53.45	53.5	53.55	53.6	53.65	53.7	53.75	53.8	53.85	53.9	53.95	54	54.05	54.1	54.15	54.2	54.25	54.3	54.35	54.4	54.45	54.5	54.55	54.6	54.65	54.7	54.75	54.8	54.85	54.9	54.95	55	55.05	55.1	55.15	55.2	55.25	55.3	55.35	55.4	55.45	55.5	55.55	55.6	55.65	55.7	55.75	55.8	55.85	55.9	55.95	56	56.05	56.1	56.15	56.2	56.25	56.3	56.35	56.4	56.45	56.5	56.55	56.6	56.65	56.7	56.75	56.8	56.85	56.9	56.95	57	57.05	57.1	57.15	57.2	57.25	57.3	57.35	57.4	57.45	57.5	57.55	57.6	57.65	57.7	57.75	57.8	57.85	57.9	57.95	58	58.05	58.1	58.15	58.2	58.25	58.3	58.35	58.4	58.45	58.5	58.55	58.6	58.65	58.7	58.75	58.8	58.85	58.9	58.95	59	59.05	59.1	59.15	59.2	59.25	59.3	59.35	59.4	59.45	59.5	59.55	59.6	59.65	59.7	59.75	59.8	59.85	59.9	59.95	60	80	72	87	88	94	77	79	91	91	86	85	89	90	109	82	89	86	98	95	92	88	90	79	96	79	105	76	106	91	112	102	94	88	93	83	85	90	94	94	117	98	89	92	99	72	109	94	101	105	102	93	87	84	88	98	96	128	85	90	111	105	95	106	117	100	95	108	86	89	102	114	116	91	100	126	106	110	106	93	120	105	100	106	91	110	93	91	88	93	114	81	99	98	109	111	107	94	86	116	108	103	86	119	94	104	93	95	105	114	107	105	91	88	115	89	104	100	115	93	100	94	106	94	73	90	92	87	95	92	110	98	110	98	89	101	99	102	87	96	93	107	98	84	111	96	108	100	98	93	106	90	107	92	97	113	88	115	93	100	93	99	107	100	94	90	110	97	110	102	87	87	102	105	92	87	93	85	96	114	87	99	103	97	89	89	86	97	88	98	100	91	107	90	90	79	88	78	87	95	109	108	124	134	153	156	127	150	123	104	95	82	88	110	93	96	101	112	107	96	119	89	106	86	101	87	104	81	103	95	108	104	87	99	100	91	124	97	95	92	105	118	94	108	111	118	97	97	92	88	89	100	92	76	88	88	73	87	100	112	82	101	86	95	102	105	97	110	100	91	105	92	103	116	99	97	91	103	102	97	94	98	96	108	100	90	119	95	102	91	88	101	93	119	97	112	104	81	90	101	101	87	92	126	95	102	83	98	109	98	100	96	107	86	123	92	99	99	103	115	118	96	95	132	94	104	99	88	112	89	94	97	103	92	94	98	116	119	110	109	98	114	125	115	103	121	110	104	112	103	118	127	130	126	111	122	131	129	137	134	127	116	122	137	99	114	153	116	129	134	120	127	139	126	153	147	158	126	161	146	201	167	158	193	169	182	177	184	159	160	151	164	144	153	123	120	151	134	123	140	136	129	124	144	121	125	128	101	122	120	98	118	98	112	95	98	118	117	93	106	98	98	117	120	104	109	116	113	99	120	119	101	109	99	121	119	124	137	96	135	115	148	109	110	113	141	159	122	134	146	159	151	184	183	175	207	235	234	238	259	266	312	299	337	380	360	432	442	402	452	437	433	409	488	453	408	389	392	376	337	321	321	336	259	276	235	228	219	192	164	182	172	150	139	141	135	133	136	116	123	114	97	102	115	102	98	106	95	91	105	89	90	84	64	82	82	95	75	68	89	75	86	72	77	75	79	87	87	81	85	79	62	83	94	77	85	72	80	75	67	73	84	84	76	81	64	75	74	60	70	76	83	78	84	82	82	96	88	96	72	79	92	86	74	97	82	74	80	66	82	83	72	62	77	71	69	74	87	81	57	71	74	70	72	81	67	74	90	63	77	78	74	64	84	70	70	59	65	57	59	71	80	65	71	59	54	90	61	54	69	71	63	73	68	74	81	75	65	72	59	93	78	58	72	52	64	80	56	61	90	62	67	78	82	67	71	60	74	69	83	73	56	60	71	57	74	80	64	71	65	69	76	61	52	67	63	91	66	74	63	57	59	59	59	75	61	82	80	55	69	60	68	69	69	61	69	59	62	71	67	87	65	78	50	75	80	54	63	57	60	60	76	68	71	62	72	60	66	79	67	64	70	64	74	64	71	65	68	64	79	74	81	78	76	83	74	88	87	73	84	86	71	85	86	95	73	91	84	73	87	92	86	85	87	77	70	78	89	77	75	89	83	87	79	76	63	72	88	55	66	64	53	71	69	83	75	62	61	66	75	55	68	63	70	72	81	70	73	62	71	86	60	58	63	65	72	94	69	64	74	92	69	67	68	78	70	70	78	79	71	77	80	66	75	69	69	67	82	84	78	79	80	MgO 10 min800 C 2 deg per min	20	20.05	20.100000000000001	20.149999999999999	20.2	20.25	20.3	20.350000000000001	20.399999999999999	20.45	20.5	20.55	20.6	20.65	20.7	20.75	20.8	20.85	20.9	20.95	21	21.05	21.1	21.15	21.2	21.25	21.3	21.35	21.4	21.45	21.5	21.55	21.6	21.65	21.7	21.75	21.8	21.85	21.9	21.95	22	22.05	22.1	22.15	22.2	22.25	22.3	22.35	22.4	22.45	22.5	22.55	22.6	22.65	22.7	22.75	22.8	22.85	22.9	22.95	23	23.05	23.1	23.15	23.2	23.25	23.3	23.35	23.4	23.45	23.5	23.55	23.6	23.65	23.7	23.75	23.8	23.85	23.9	23.95	24	24.05	24.1	24.15	24.2	24.25	24.3	24.35	24.4	24.45	24.5	24.55	24.6	24.65	24.7	24.75	24.8	24.85	24.9	24.95	25	25.05	25.1	25.15	25.2	25.25	25.3	25.35	25.4	25.45	25.5	25.55	25.6	25.65	25.7	25.75	25.8	25.85	25.9	25.95	26	26.05	26.1	26.15	26.2	26.25	26.3	26.35	26.4	26.45	26.5	26.55	26.6	26.65	26.7	26.75	26.8	26.85	26.9	26.95	27	27.05	27.1	27.15	27.2	27.25	27.3	27.35	27.4	27.45	27.5	27.55	27.6	27.65	27.7	27.75	27.8	27.85	27.9	27.95	28	28.05	28.1	28.15	28.2	28.25	28.3	28.35	28.4	28.45	28.5	28.55	28.6	28.65	28.7	28.75	28.8	28.85	28.9	28.95	29	29.05	29.1	29.15	29.2	29.25	29.3	29.35	29.4	29.45	29.5	29.55	29.6	29.65	29.7	29.75	29.8	29.85	29.9	29.95	30	30.05	30.1	30.15	30.2	30.25	30.3	30.35	30.4	30.45	30.5	30.55	30.6	30.65	30.7	30.75	30.8	30.85	30.9	30.95	31	31.05	31.1	31.15	31.2	31.25	31.3	31.35	31.4	31.45	31.5	31.55	31.6	31.65	31.7	31.75	31.8	31.85	31.9	31.95	32	32.049999999999997	32.1	32.15	32.200000000000003	32.25	32.299999999999997	32.35	32.4	32.450000000000003	32.5	32.549999999999997	32.6	32.65	32.700000000000003	32.75	32.799999999999997	32.85	32.9	32.950000000000003	33	33.049999999999997	33.1	33.15	33.200000000000003	33.25	33.299999999999997	33.35	33.4	33.450000000000003	33.5	33.549999999999997	33.6	33.65	33.700000000000003	33.75	33.799999999999997	33.85	33.9	33.950000000000003	34	34.049999999999997	34.1	34.15	34.200000000000003	34.25	34.299999999999997	34.35	34.4	34.450000000000003	34.5	34.549999999999997	34.6	34.65	34.700000000000003	34.75	34.799999999999997	34.85	34.9	34.950000000000003	35	35.049999999999997	35.1	35.15	35.200000000000003	35.25	35.299999999999997	35.35	35.4	35.450000000000003	35.5	35.549999999999997	35.6	35.65	35.700000000000003	35.75	35.799999999999997	35.85	35.9	35.950000000000003	36	36.049999999999997	36.1	36.15	36.200000000000003	36.25	36.299999999999997	36.35	36.4	36.450000000000003	36.5	36.549999999999997	36.6	36.65	36.700000000000003	36.75	36.799999999999997	36.85	36.9	36.950000000000003	37	37.049999999999997	37.1	37.15	37.200000000000003	37.25	37.299999999999997	37.35	37.4	37.450000000000003	37.5	37.549999999999997	37.6	37.65	37.700000000000003	37.75	37.799999999999997	37.85	37.9	37.950000000000003	38	38.049999999999997	38.1	38.15	38.200000000000003	38.25	38.299999999999997	38.35	38.4	38.450000000000003	38.5	38.549999999999997	38.6	38.65	38.700000000000003	38.75	38.799999999999997	38.85	38.9	38.950000000000003	39	39.049999999999997	39.1	39.15	39.200000000000003	39.25	39.299999999999997	39.35	39.4	39.450000000000003	39.5	39.549999999999997	39.6	39.65	39.700000000000003	39.75	39.799999999999997	39.85	39.9	39.950000000000003	40	40.049999999999997	40.1	40.15	40.200000000000003	40.25	40.299999999999997	40.35	40.4	40.450000000000003	40.5	40.549999999999997	40.6	40.65	40.700000000000003	40.75	40.799999999999997	40.85	40.9	40.950000000000003	41	41.05	41.1	41.15	41.2	41.25	41.3	41.35	41.4	41.45	41.5	41.55	41.6	41.65	41.7	41.75	41.8	41.85	41.9	41.95	42	42.05	42.1	42.15	42.2	42.25	42.3	42.35	42.4	42.45	42.5	42.55	42.6	42.65	42.7	42.75	42.8	42.85	42.9	42.95	43	43.05	43.1	43.15	43.2	43.25	43.3	43.35	43.4	43.45	43.5	43.55	43.6	43.65	43.7	43.75	43.8	43.85	43.9	43.95	44	44.05	44.1	44.15	44.2	44.25	44.3	44.35	44.4	44.45	44.5	44.55	44.6	44.65	44.7	44.75	44.8	44.85	44.9	44.95	45	45.05	45.1	45.15	45.2	45.25	45.3	45.35	45.4	45.45	45.5	45.55	45.6	45.65	45.7	45.75	45.8	45.85	45.9	45.95	46	46.05	46.1	46.15	46.2	46.25	46.3	46.35	46.4	46.45	46.5	46.55	46.6	46.65	46.7	46.75	46.8	46.85	46.9	46.95	47	47.05	47.1	47.15	47.2	47.25	47.3	47.35	47.4	47.45	47.5	47.55	47.6	47.65	47.7	47.75	47.8	47.85	47.9	47.95	48	48.05	48.1	48.15	48.2	48.25	48.3	48.35	48.4	48.45	48.5	48.55	48.6	48.65	48.7	48.75	48.8	48.85	48.9	48.95	49	49.05	49.1	49.15	49.2	49.25	49.3	49.35	49.4	49.45	49.5	49.55	49.6	49.65	49.7	49.75	49.8	49.85	49.9	49.95	50	50.05	50.1	50.15	50.2	50.25	50.3	50.35	50.4	50.45	50.5	50.55	50.6	50.65	50.7	50.75	50.8	50.85	50.9	50.95	51	51.05	51.1	51.15	51.2	51.25	51.3	51.35	51.4	51.45	51.5	51.55	51.6	51.65	51.7	51.75	51.8	51.85	51.9	51.95	52	52.05	52.1	52.15	52.2	52.25	52.3	52.35	52.4	52.45	52.5	52.55	52.6	52.65	52.7	52.75	52.8	52.85	52.9	52.95	53	53.05	53.1	53.15	53.2	53.25	53.3	53.35	53.4	53.45	53.5	53.55	53.6	53.65	53.7	53.75	53.8	53.85	53.9	53.95	54	54.05	54.1	54.15	54.2	54.25	54.3	54.35	54.4	54.45	54.5	54.55	54.6	54.65	54.7	54.75	54.8	54.85	54.9	54.95	55	55.05	55.1	55.15	55.2	55.25	55.3	55.35	55.4	55.45	55.5	55.55	55.6	55.65	55.7	55.75	55.8	55.85	55.9	55.95	56	56.05	56.1	56.15	56.2	56.25	56.3	56.35	56.4	56.45	56.5	56.55	56.6	56.65	56.7	56.75	56.8	56.85	56.9	56.95	57	57.05	57.1	57.15	57.2	57.25	57.3	57.35	57.4	57.45	57.5	57.55	57.6	57.65	57.7	57.75	57.8	57.85	57.9	57.95	58	58.05	58.1	58.15	58.2	58.25	58.3	58.35	58.4	58.45	58.5	58.55	58.6	58.65	58.7	58.75	58.8	58.85	58.9	58.95	59	59.05	59.1	59.15	59.2	59.25	59.3	59.35	59.4	59.45	59.5	59.55	59.6	59.65	59.7	59.75	59.8	59.85	59.9	59.95	60	60	63	79	60	54	64	64	54	54	70	61	78	64	63	72	53	77	82	75	73	74	64	79	72	83	55	79	67	67	75	87	63	92	71	70	76	75	70	85	77	88	62	72	82	71	56	72	63	81	78	72	64	75	76	74	99	83	73	81	77	82	72	77	64	72	75	70	80	76	80	85	90	79	111	102	81	90	112	103	86	82	80	82	72	75	74	73	90	78	78	64	63	79	78	83	75	97	80	64	81	83	76	77	85	67	80	73	96	78	84	70	68	96	81	81	77	73	62	90	76	82	71	68	85	56	87	71	74	90	67	52	70	76	73	78	76	90	73	74	68	83	68	82	57	75	87	85	60	68	65	58	71	71	73	72	81	77	84	81	74	73	84	74	74	63	68	79	67	68	93	78	72	74	71	77	75	65	77	70	69	72	59	81	82	83	78	59	82	68	78	89	80	66	69	64	69	87	68	69	77	68	82	79	70	84	72	77	60	77	68	81	73	77	63	64	87	76	72	75	75	85	79	80	72	79	52	66	63	66	87	81	96	76	67	73	70	80	81	75	81	75	76	74	55	65	68	64	78	63	78	82	73	100	76	68	90	65	61	73	80	75	71	82	77	72	59	67	74	81	74	66	61	78	65	71	65	81	79	85	79	69	92	87	77	83	84	92	83	82	76	94	84	89	58	77	58	63	80	71	80	69	78	65	76	85	82	80	76	87	87	87	85	68	75	76	67	74	65	77	81	70	90	74	78	84	90	74	91	71	76	70	68	76	76	73	63	77	95	79	74	79	87	78	76	101	92	108	79	89	78	109	92	106	120	106	113	115	112	105	94	101	107	87	95	99	94	78	70	84	85	77	97	97	88	90	118	108	104	125	126	118	108	126	148	165	162	151	153	179	160	155	147	150	132	121	125	104	121	115	106	89	85	93	88	90	105	81	73	73	93	71	80	91	77	81	77	67	77	71	69	72	80	73	66	74	68	67	60	54	66	74	82	72	81	65	85	77	82	91	93	67	84	84	100	95	86	78	74	92	104	105	127	123	112	120	135	117	154	153	170	192	188	231	266	283	312	322	382	410	431	494	475	500	589	536	565	558	532	516	481	424	384	347	306	271	236	224	190	176	145	123	124	116	90	93	92	107	92	91	74	93	84	99	66	76	80	71	80	71	70	53	59	60	72	85	60	61	64	68	65	71	73	68	49	62	60	65	69	47	72	55	53	61	66	66	59	57	70	59	62	53	59	70	58	60	54	59	58	65	68	59	53	51	61	65	72	64	56	64	56	46	46	60	64	51	52	68	51	64	61	50	64	63	64	62	62	50	58	45	57	62	54	57	60	47	65	62	58	64	71	46	53	60	50	62	57	59	58	57	54	56	52	48	56	43	45	62	47	57	47	56	52	59	53	47	54	65	54	55	61	66	52	60	46	63	60	45	58	64	45	48	60	59	67	66	51	54	61	57	67	63	49	50	55	36	65	65	58	64	49	45	34	41	50	53	51	52	49	60	55	51	62	38	57	45	41	50	60	54	50	47	49	57	46	53	51	65	63	51	45	50	58	48	57	57	55	51	52	54	72	63	67	52	69	55	47	52	58	42	50	56	59	54	54	50	65	47	58	60	53	51	59	54	47	53	59	64	79	77	77	81	83	101	75	89	76	84	88	91	99	87	93	91	104	81	86	69	73	65	86	66	79	51	56	67	55	61	56	60	45	62	60	42	66	58	45	42	67	52	57	49	51	48	54	67	47	57	63	65	45	48	52	37	45	46	53	59	56	58	55	53	49	50	59	53	45	64	72	41	56	65	48	54	68	54	59	55	52	51	51	55	2θ


tensity





	Sample time (min)	Diameter (nano meter)
	5	2.679652
 
	10	2.602733
 
	20	1.210166
 

Table(2): MgO time series at 600 c and 2deg per min



Figure(2):MgO time series @600 c and 2deg per min


MgO time series 
5 min	20	20.05	20.100000000000001	20.149999999999999	20.2	20.25	20.3	20.350000000000001	20.399999999999999	20.45	20.5	20.55	20.6	20.65	20.7	20.75	20.8	20.85	20.9	20.95	21	21.05	21.1	21.15	21.2	21.25	21.3	21.35	21.4	21.45	21.5	21.55	21.6	21.65	21.7	21.75	21.8	21.85	21.9	21.95	22	22.05	22.1	22.15	22.2	22.25	22.3	22.35	22.4	22.45	22.5	22.55	22.6	22.65	22.7	22.75	22.8	22.85	22.9	22.95	23	23.05	23.1	23.15	23.2	23.25	23.3	23.35	23.4	23.45	23.5	23.55	23.6	23.65	23.7	23.75	23.8	23.85	23.9	23.95	24	24.05	24.1	24.15	24.2	24.25	24.3	24.35	24.4	24.45	24.5	24.55	24.6	24.65	24.7	24.75	24.8	24.85	24.9	24.95	25	25.05	25.1	25.15	25.2	25.25	25.3	25.35	25.4	25.45	25.5	25.55	25.6	25.65	25.7	25.75	25.8	25.85	25.9	25.95	26	26.05	26.1	26.15	26.2	26.25	26.3	26.35	26.4	26.45	26.5	26.55	26.6	26.65	26.7	26.75	26.8	26.85	26.9	26.95	27	27.05	27.1	27.15	27.2	27.25	27.3	27.35	27.4	27.45	27.5	27.55	27.6	27.65	27.7	27.75	27.8	27.85	27.9	27.95	28	28.05	28.1	28.15	28.2	28.25	28.3	28.35	28.4	28.4	5	28.5	28.55	28.6	28.65	28.7	28.75	28.8	28.85	28.9	28.95	29	29.05	29.1	29.15	29.2	29.25	29.3	29.35	29.4	29.45	29.5	29.55	29.6	29.65	29.7	29.75	29.8	29.85	29.9	29.95	30	30.05	30.1	30.15	30.2	30.25	30.3	30.35	30.4	30.45	30.5	30.55	30.6	30.65	30.7	30.75	30.8	30.85	30.9	30.95	31	31.05	31.1	31.15	31.2	31.25	31.3	31.35	31.4	31.45	31.5	31.55	31.6	31.65	31.7	31.75	31.8	31.85	31.9	31.95	32	32.049999999999997	32.1	32.15	32.200000000000003	32.25	32.299999999999997	32.35	32.4	32.450000000000003	32.5	32.549999999999997	32.6	32.65	32.700000000000003	32.75	32.799999999999997	32.85	32.9	32.950000000000003	33	33.049999999999997	33.1	33.15	33.200000000000003	33.25	33.299999999999997	33.35	33.4	33.450000000000003	33.5	33.549999999999997	33.6	33.65	33.700000000000003	33.75	33.799999999999997	33.85	33.9	33.950000000000003	34	34.049999999999997	34.1	34.15	34.200000000000003	34.25	34.299999999999997	34.35	34.4	34.450000000000003	34.5	34.549999999999997	34.6	34.65	34.700000000000003	34.75	34.799999999999997	34.85	34.9	34.950000000000003	35	35.049999999999997	35.1	35.15	35.200000000000003	35.25	35.299999999999997	35.35	35.4	35.450000000000003	35.5	35.549999999999997	35.6	35.65	35.700000000000003	35.75	35.799999999999997	35.85	35.9	35.950000000000003	36	36.049999999999997	36.1	36.15	36.200000000000003	36.25	36.299999999999997	36.35	36.4	36.450000000000003	36.5	36.549999999999997	36.6	36.65	36.700000000000003	36.75	36.799999999999997	36.85	36.9	36.950000000000003	37	37.049999999999997	37.1	37.15	37.200000000000003	37.25	37.299999999999997	37.35	37.4	37.450000000000003	37.5	37.549999999999997	37.6	37.65	37.700000000000003	37.75	37.799999999999997	37.85	37.9	37.950000000000003	38	38.049999999999997	38.1	38.15	38.200000000000003	38.25	38.299999999999997	38.35	38.4	38.450000000000003	38.5	38.549999999999997	38.6	38.65	38.700000000000003	38.75	38.799999999999997	38.85	38.9	38.950000000000003	39	39.049999999999997	39.1	39.15	39.200000000000003	39.25	39.299999999999997	39.35	39.4	39.450000000000003	39.5	39.549999999999997	39.6	39.65	39.700000000000003	39.75	39.799999999999997	39.85	39.9	39.950000000000003	40	40.049999999999997	40.1	40.15	40.200000000000003	40.25	40.299999999999997	40.35	40.4	40.450000000000003	40.5	40.549999999999997	40.6	40.65	40.700000000000003	40.75	40.799999999999997	40.85	40.9	40.950000000000003	41	41.05	41.1	41.15	41.2	41.25	41.3	41.35	41.4	41.45	41.5	41.55	41.6	41.65	41.7	41.75	41.8	41.85	41.9	41.95	42	42.05	42.1	42.15	42.2	42.25	42.3	42.35	42.4	42.45	42.5	42.55	42.6	42.65	42.7	42.75	42.8	42.85	42.9	42.95	43	43.05	43.1	43.15	43.2	43.25	43.3	43.35	43.4	43.45	43.5	43.55	43.6	43.65	43.7	43.75	43.8	43.85	43.9	43.95	44	44.05	44.1	44.15	44.2	44.25	44.3	44.35	44.4	44.45	44.5	44.55	44.6	44.65	44.7	44.75	44.8	44.85	44.9	44.95	45	45.05	45.1	45.15	45.2	45.25	45.3	45.35	45.4	45.45	45.5	45.55	45.6	45.65	45.7	45.75	45.8	45	.85	45.9	45.95	46	46.05	46.1	46.15	46.2	46.25	46.3	46.35	46.4	46.45	46.5	46.55	46.6	46.65	46.7	46.75	46.8	46.85	46.9	46.95	47	47.05	47.1	47.15	47.2	47.25	47.3	47.35	47.4	47.45	47.5	47.55	47.6	47.65	47.7	47.75	47.8	47.85	47.9	47.95	48	48.05	48.1	48.15	48.2	48.25	48.3	48.35	48.4	48.45	48.5	48.55	48.6	48.65	48.7	48.75	48.8	48.85	48.9	48.95	49	49.05	49.1	49.15	49.2	49.25	49.3	49.35	49.4	49.45	49.5	49.55	49.6	49.65	49.7	49.75	49.8	49.85	49.9	49.95	50	50.05	50.1	50.15	50.2	50.25	50.3	50.35	50.4	50.45	50.5	50.55	50.6	50.65	50.7	50.75	50.8	50.85	50.9	50.95	51	51.05	51.1	51.15	51.2	51.25	51.3	51.35	51.4	51.45	51.5	51.55	51.6	51.65	51.7	51.75	51.8	51.85	51.9	51.95	52	52.05	52.1	52.15	52.2	52.25	52.3	52.35	52.4	52.45	52.5	52.55	52.6	52.65	52.7	52.75	52.8	52.85	52.9	52.95	53	53.05	53.1	53.15	53.2	53.25	53.3	53.35	53.4	53.45	53.5	53.55	53.6	53.65	53.7	53.75	53.8	53.85	53.9	53.95	54	54.05	54.1	54.15	54.2	54.25	54.3	54.35	54.4	54.45	54.5	54.55	54.6	54.65	54.7	54.75	54.8	54.85	54.9	54.95	55	55.05	55.1	55.15	55.2	55.25	55.3	55.35	55.4	55.45	55.5	55.55	55.6	55.65	55.7	55.75	55.8	55.85	55.9	55.95	56	56.05	56.1	56.15	56.2	56.25	56.3	56.35	56.4	56.45	56.5	56.55	56.6	56.65	56.7	56.75	56.8	56.85	56.9	56.95	57	57.05	57.1	57.15	57.2	57.25	57.3	57.35	57.4	57.45	57.5	57.55	57.6	57.65	57.7	57.75	57.8	57.85	57.9	57.95	58	58.05	58.1	58.15	58.2	58.25	58.3	58.35	58.4	58.45	58.5	58.55	58.6	58.65	58.7	58.75	58.8	58.85	58.9	58.95	59	59.05	59.1	59.15	59.2	59.25	59.3	59.35	59.4	59.45	59.5	59.55	59.6	59.65	59.7	59.75	59.8	59.85	59.9	59.95	60	80	84	71	74	72	75	79	79	87	91	83	76	92	84	99	81	72	68	82	85	93	98	96	81	96	82	106	93	94	72	88	87	93	95	84	91	91	86	87	94	85	85	90	91	86	76	95	90	86	89	101	78	111	83	100	102	83	92	92	119	95	94	84	104	103	79	107	96	103	117	92	121	125	104	114	94	108	107	119	112	96	97	93	91	111	84	98	86	98	102	113	103	94	99	91	92	108	103	75	97	110	87	94	80	97	70	107	75	96	88	95	98	106	102	97	108	90	95	92	103	90	105	95	94	107	95	126	98	105	105	80	92	101	100	82	95	97	97	75	98	95	99	90	96	99	100	95	88	99	96	88	94	93	109	102	93	92	107	100	113	84	93	90	101	93	113	94	86	104	78	101	94	105	94	74	84	89	87	102	78	96	101	72	97	97	88	100	91	96	92	101	99	84	81	87	97	97	78	85	100	98	95	82	105	102	96	107	114	97	111	106	97	93	90	107	89	90	93	87	101	102	79	102	109	94	87	89	92	91	75	98	77	91	89	92	82	88	97	91	85	102	97	76	75	86	92	85	94	95	87	106	83	85	89	95	84	79	85	88	77	106	80	100	98	114	107	95	103	116	97	100	104	108	98	113	87	81	91	101	88	89	79	103	89	68	83	93	89	87	88	70	78	78	85	104	84	86	82	71	122	81	72	73	83	89	82	92	77	88	71	87	90	81	92	71	86	95	92	79	77	91	79	85	80	93	85	75	75	86	101	95	101	94	89	89	102	91	94	93	86	102	90	86	80	92	94	100	80	97	97	80	89	100	91	82	95	83	79	82	94	91	87	91	85	99	90	100	82	97	95	107	90	83	97	96	86	95	96	94	102	103	107	108	84	85	119	99	95	120	93	102	87	109	87	90	81	84	99	81	93	97	97	84	92	109	80	82	91	109	88	82	76	64	102	101	80	78	93	82	101	88	83	74	90	85	73	101	89	83	89	97	92	100	94	86	90	92	98	99	107	90	88	104	93	104	84	79	88	117	123	127	128	94	124	139	114	129	131	128	135	145	184	134	152	165	165	156	163	174	178	191	159	197	197	202	191	190	186	189	187	166	172	158	167	149	119	137	140	146	128	107	131	122	119	130	123	101	82	102	108	93	102	92	85	80	94	98	94	77	86	76	82	76	82	65	71	86	69	91	81	69	82	68	80	74	69	63	67	72	74	72	89	74	80	84	63	87	69	69	65	72	56	64	72	76	52	63	68	87	80	69	92	72	78	73	81	62	69	76	75	57	59	67	61	69	48	79	63	57	77	65	81	71	75	62	58	57	60	79	57	65	79	62	58	69	62	68	71	67	81	59	62	61	74	70	65	63	55	63	55	61	61	53	66	57	53	66	59	58	64	58	58	59	63	77	66	66	63	52	72	57	82	61	75	62	72	54	62	65	54	69	61	58	65	80	70	56	57	63	65	57	75	65	59	63	59	66	61	56	62	62	46	78	60	65	64	65	50	55	62	50	60	65	80	41	62	55	56	56	64	57	71	49	48	60	65	57	60	58	57	55	65	74	71	46	70	60	74	61	69	81	73	68	67	56	83	63	67	56	65	73	53	68	66	55	53	54	69	55	69	63	56	58	72	50	71	71	75	81	55	65	55	70	73	73	59	68	68	85	82	65	72	67	72	66	67	76	71	66	63	57	76	66	70	66	63	58	57	59	69	60	59	51	69	58	55	68	63	61	64	70	61	68	72	62	56	64	73	67	70	66	66	76	59	54	59	62	55	60	54	53	48	57	64	52	57	65	63	65	59	45	52	57	54	51	81	57	64	75	60	48	10 min	20	20.05	20.100000000000001	20.149999999999999	20.2	20.25	20.3	20.350000000000001	20.399999999999999	20.45	20.5	20.55	20.6	20.65	20.7	20.75	20.8	20.85	20.9	20.95	21	21.05	21.1	21.15	21.2	21.25	21.3	21.35	21.4	21.45	21.5	21.55	21.6	21.65	21.7	21.75	21.8	21.85	21.9	21.95	22	22.05	22.1	22.15	22.2	22.25	22.3	22.35	22.4	22.45	22.5	22.55	22.6	22.65	22.7	22.75	22.8	22.85	22.9	22.95	23	23.05	23.1	23.15	23.2	23.25	23.3	23.35	23.4	23.45	23.5	23.55	23.6	23.65	23.7	23.75	23.8	23.85	23.9	23.95	24	24.05	24.1	24.15	24.2	24.25	24.3	24.35	24.4	24.45	24.5	24.55	24.6	24.65	24.7	24.75	24.8	24.85	24.9	24.95	25	25.05	25.1	25.15	25.2	25.25	25.3	25.35	25.4	25.45	25.5	25.55	25.6	25.65	25.7	25.75	25.8	25.85	25.9	25.95	26	26.05	26.1	26.15	26.2	26.25	26.3	26.35	26.4	26.45	26.5	26.55	26.6	26.65	26.7	26.75	26.8	26.85	26.9	26.95	27	27.05	27.1	27.15	27.2	27.25	27.3	27.35	27.4	27.45	27.5	27.55	27.6	27.65	27.7	27.75	27.8	27.85	27.9	27.95	28	28.05	28.1	28.15	28.2	28.25	28.3	28.35	28.4	28.45	28.5	28.55	28.6	28.65	28.7	28.75	28.8	28	.85	28.9	28.95	29	29.05	29.1	29.15	29.2	29.25	29.3	29.35	29.4	29.45	29.5	29.55	29.6	29.65	29.7	29.75	29.8	29.85	29.9	29.95	30	30.05	30.1	30.15	30.2	30.25	30.3	30.35	30.4	30.45	30.5	30.55	30.6	30.65	30.7	30.75	30.8	30.85	30.9	30.95	31	31.05	31.1	31.15	31.2	31.25	31.3	31.35	31.4	31.45	31.5	31.55	31.6	31.65	31.7	31.75	31.8	31.85	31.9	31.95	32	32.049999999999997	32.1	32.15	32.200000000000003	32.25	32.299999999999997	32.35	32.4	32.450000000000003	32.5	32.549999999999997	32.6	32.65	32.700000000000003	32.75	32.799999999999997	32.85	32.9	32.950000000000003	33	33.049999999999997	33.1	33.15	33.200000000000003	33.25	33.299999999999997	33.35	33.4	33.450000000000003	33.5	33.549999999999997	33.6	33.65	33.700000000000003	33.75	33.799999999999997	33.85	33.9	33.950000000000003	34	34.049999999999997	34.1	34.15	34.200000000000003	34.25	34.299999999999997	34.35	34.4	34.450000000000003	34.5	34.549999999999997	34.6	34.65	34.700000000000003	34.75	34.799999999999997	34.85	34.9	34.950000000000003	35	35.049999999999997	35.1	35.15	35.200000000000003	35.25	35.299999999999997	35.35	35.4	35.450000000000003	35.5	35.549999999999997	35.6	35.65	35.700000000000003	35.75	35.799999999999997	35.85	35.9	35.950000000000003	36	36.049999999999997	36.1	36.15	36.200000000000003	36.25	36.299999999999997	36.35	36.4	36.450000000000003	36.5	36.549999999999997	36.6	36.65	36.700000000000003	36.75	36.799999999999997	36.85	36.9	36.950000000000003	37	37.049999999999997	37.1	37.15	37.200000000000003	37.25	37.299999999999997	37.35	37.4	37.450000000000003	37.5	37.549999999999997	37.6	37.65	37.700000000000003	37.75	37.799999999999997	37.85	37.9	37.950000000000003	38	38.049999999999997	38.1	38.15	38.200000000000003	38.25	38.299999999999997	38.35	38.4	38.450000000000003	38.5	38.549999999999997	38.6	38.65	38.700000000000003	38.75	38.799999999999997	38.85	38.9	38.950000000000003	39	39.049999999999997	39.1	39.15	39.200000000000003	39.25	39.299999999999997	39.35	39.4	39.450000000000003	39.5	39.549999999999997	39.6	39.65	39.700000000000003	39.75	39.799999999999997	39.85	39.9	39.950000000000003	40	40.049999999999997	40.1	40.15	40.200000000000003	40.25	40.299999999999997	40.35	40.4	40.450000000000003	40.5	40.549999999999997	40.6	40.65	40.700000000000003	40.75	40.799999999999997	40.85	40.9	40.950000000000003	41	41.05	41.1	41.15	41.2	41.25	41.3	41.35	41.4	41.45	41.5	41.55	41.6	41.65	41.7	41.75	41.8	41.85	41.9	41.95	42	42.05	42.1	42.15	42.2	42.25	42.3	42.35	42.4	42.45	42.5	42.55	42.6	42.65	42.7	42.75	42.8	42.85	42.9	42.95	43	43.05	43.1	43.15	43.2	43.25	43.3	43.35	43.4	43.45	43.5	43.55	43.6	43.65	43.7	43.75	43.8	43.85	43.9	43.95	44	44.05	44.1	44.15	44.2	44.25	44.3	44.35	44.4	44.45	44.5	44.55	44.6	44.65	44.7	44.75	44.8	44.85	44.9	44.95	45	45.05	45.1	45.15	45.2	45.25	45.3	45.35	45.4	45.45	45.5	45.55	45.6	45.65	45.7	45.75	45.8	45.85	45.9	45.95	46	46.05	46.1	46.15	46.2	46.25	46.3	46.35	46.4	46.45	46.5	46.55	46.6	46.65	46.7	46.75	46.8	46.85	46.9	46.95	47	47.05	47.1	47.15	47.2	47.25	47.3	47.35	47.4	47.45	47.5	47.55	47.6	47.65	47.7	47.75	47.8	47.85	47.9	47.95	48	48.05	48.1	48.15	48.2	48.25	48.3	48.35	48.4	48.45	48.5	48.55	48.6	48.65	48.7	48.75	48.8	48.85	48.9	48.95	49	49.05	49.1	49.15	49.2	49.25	49.3	49.35	49.4	49.45	49.5	49.55	49.6	49.65	49.7	49.75	49.8	49.85	49.9	49.95	50	50.05	50.1	50.15	50.2	50.25	50.3	50.35	50.4	50.45	50.5	50.55	50.6	50.65	50.7	50.75	50.8	50.85	50.9	50.95	51	51.05	51.1	51.15	51.2	51.25	51.3	51.35	51.4	51.45	51.5	51.55	51.6	51.65	51.7	51.75	51.8	51.85	51.9	51.95	52	52.05	52.1	52.15	52.2	52.25	52.3	52.35	52.4	52.45	52.5	52.55	52.6	52.65	52.7	52.75	52.8	52.85	52.9	52.95	53	53.05	53.1	53.15	53.2	53.25	53.3	53.35	53.4	53.45	53.5	53.55	53.6	53.65	53.7	53.75	53.8	53.85	53.9	53.95	54	54.05	54.1	54.15	54.2	54.25	54.3	54.35	54.4	54.45	54.5	54.55	54.6	54.65	54.7	54.75	54.8	54.85	54.9	54.95	55	55.05	55.1	55.15	55.2	55.25	55.3	55.35	55.4	55.45	55.5	55.55	55.6	55.65	55.7	55.75	55.8	55.85	55.9	55.95	56	56.05	56.1	56.15	56.2	56.25	56.3	56.35	56.4	56.45	56.5	56.55	56.6	56.65	56.7	56.75	56.8	56.85	56.9	56.95	57	57.05	57.1	57.15	57.2	57.25	57.3	57.35	57.4	57.45	57.5	57.55	57.6	57.65	57.7	57.75	57.8	57.85	57.9	57.95	58	58.05	58.1	58.15	58.2	58.25	58.3	58.35	58.4	58.45	58.5	58.55	58.6	58.65	58.7	58.75	58.8	58.85	58.9	58.95	59	59.05	59.1	59.15	59.2	59.25	59.3	59.35	59.4	59.45	59.5	59.55	59.6	59.65	59.7	59.75	59.8	59.85	59.9	59.95	60	117	112	108	106	127	108	99	111	112	115	101	100	139	110	134	115	105	101	104	104	120	119	109	102	93	110	114	96	120	92	114	108	113	110	114	104	93	98	99	109	112	111	97	122	113	93	97	93	102	129	95	110	106	117	125	119	97	121	137	120	111	114	133	121	118	151	119	134	106	130	142	119	123	122	138	115	122	120	116	123	124	100	110	109	103	99	117	112	122	125	103	118	116	101	113	113	96	123	111	122	106	104	107	104	115	126	115	115	108	108	111	99	99	100	110	109	103	113	100	130	105	99	131	126	107	122	114	107	103	109	102	123	101	126	102	126	100	96	104	97	96	112	108	120	125	112	122	120	113	119	106	108	111	109	132	111	120	104	107	120	87	93	130	114	104	119	100	108	101	120	91	100	109	95	107	120	115	123	119	124	103	121	121	123	108	107	126	108	104	112	102	138	109	112	108	130	138	122	126	112	143	152	141	143	158	170	131	125	135	135	105	11	5	133	110	105	102	123	114	134	121	103	104	109	100	102	115	130	115	98	93	118	88	122	107	108	113	98	122	101	120	121	117	93	119	119	125	109	118	113	102	125	109	93	106	100	129	110	135	92	127	117	101	96	98	104	112	121	124	133	126	126	122	101	109	119	100	116	113	108	115	121	119	129	109	106	128	127	115	114	123	126	131	115	133	112	124	118	110	127	129	119	110	125	122	127	125	127	119	135	118	96	111	113	106	110	136	150	138	132	118	119	107	126	153	125	130	117	111	119	118	131	133	132	126	132	140	139	157	158	147	128	142	135	129	129	147	148	151	125	140	141	155	163	155	148	143	154	168	122	153	174	139	166	178	174	170	170	180	173	166	168	168	190	171	203	189	207	201	198	193	197	190	199	173	187	182	208	176	212	186	168	186	140	168	166	165	150	145	143	158	138	137	158	153	147	145	136	132	130	154	158	137	125	109	127	117	130	114	139	109	113	144	165	120	121	125	117	118	147	133	143	134	122	126	117	139	122	139	143	132	163	154	160	159	134	205	175	184	178	168	210	195	235	197	225	263	260	276	272	282	311	342	336	336	328	371	370	359	377	370	394	382	354	358	356	353	341	338	295	273	278	291	256	222	221	207	205	208	196	157	163	120	183	161	158	157	150	108	134	123	121	144	129	120	117	144	144	120	125	115	92	129	106	100	82	106	98	98	110	122	109	95	76	99	88	109	77	83	105	96	88	104	104	106	101	108	93	82	86	83	77	87	86	85	87	81	98	88	88	88	107	97	83	89	80	77	84	86	104	94	86	84	76	90	90	102	111	93	94	97	104	101	72	90	78	106	89	81	87	88	81	92	72	92	81	76	88	96	81	95	95	94	94	94	87	93	76	86	84	77	79	82	87	71	76	81	76	80	85	85	67	89	70	70	74	78	74	97	76	75	76	100	79	94	79	66	77	76	89	91	64	93	66	86	90	80	83	91	77	84	86	107	68	86	70	96	85	80	85	67	85	99	77	75	71	80	88	82	80	77	81	71	86	83	80	92	95	74	68	79	61	70	84	63	76	69	84	84	60	81	71	79	90	75	70	61	71	67	88	85	88	74	70	76	77	84	77	90	80	80	70	72	88	88	79	79	97	75	71	89	91	80	93	93	94	102	100	106	84	90	108	90	89	90	85	98	86	102	79	86	105	88	81	84	104	81	109	95	83	87	87	84	94	102	96	80	84	84	77	91	69	86	94	81	89	77	86	85	79	84	71	76	69	60	93	62	86	80	84	92	63	88	75	86	78	74	77	73	82	100	75	96	92	95	97	82	96	91	113	87	82	82	100	105	96	80	91	100	86	90	80	20 min	20	20.05	20.100000000000001	20.149999999999999	20.2	20.25	20.3	20.350000000000001	20.399999999999999	20.45	20.5	20.55	20.6	20.65	20.7	20.75	20.8	20.85	20.9	20.95	21	21.05	21.1	21.15	21.2	21.25	21.3	21.35	21.4	21.45	21.5	21.55	21.6	21.65	21.7	21.75	21.8	21.85	21.9	21.95	22	22.05	22.1	22.15	22.2	22.25	22.3	22.35	22.4	22.45	22.5	22.55	22.6	22.65	22.7	22.75	22.8	22.85	22.9	22.95	23	23.05	23.1	23.15	23.2	23.25	23.3	23.35	23.4	23.45	23.5	23.55	23.6	23.65	23.7	23.75	23.8	23.85	23.9	23.95	24	24.05	24.1	24.15	24.2	24.25	24.3	24.35	24.4	24.45	24.5	24.55	24.6	24.65	24.7	24.75	24.8	24.85	24.9	24.95	25	25.05	25.1	25.15	25.2	25.25	25.3	25.35	25.4	25.45	25.5	25.55	25.6	25.65	25.7	25.75	25.8	25.85	25.9	25.95	26	26.05	26.1	26.15	26.2	26.25	26.3	26.35	26.4	26.45	26.5	26.55	26.6	26.65	26.7	26.75	26.8	26.85	26.9	26.95	27	27.05	27.1	27.15	27.2	27.25	27.3	27.35	27.4	27.45	27.5	27.55	27.6	27.65	27.7	27.75	27.8	27.85	27.9	27.95	28	28.05	28.1	28.15	28.2	28.25	28.3	28.35	28.4	28.45	28.5	28.55	28.6	28.65	28.7	28.75	28.8	28.85	28.9	28.95	29	29.05	29.1	29.15	29.2	29.25	29.3	29.35	29.4	29.45	29.5	29.55	29.6	29.65	29.7	29.75	29.8	29.85	29.9	29.95	30	30.05	30.1	30.15	30.2	30.25	30.3	30.35	30.4	30.45	30.5	30.55	30.6	30.65	30.7	30.75	30.8	30.85	30.9	30.95	31	31.05	31.1	31.15	31.2	31.25	31.3	31.35	31.4	31.4	5	31.5	31.55	31.6	31.65	31.7	31.75	31.8	31.85	31.9	31.95	32	32.049999999999997	32.1	32.15	32.200000000000003	32.25	32.299999999999997	32.35	32.4	32.450000000000003	32.5	32.549999999999997	32.6	32.65	32.700000000000003	32.75	32.799999999999997	32.85	32.9	32.950000000000003	33	33.049999999999997	33.1	33.15	33.200000000000003	33.25	33.299999999999997	33.35	33.4	33.450000000000003	33.5	33.549999999999997	33.6	33.65	33.700000000000003	33.75	33.799999999999997	33.85	33.9	33.950000000000003	34	34.049999999999997	34.1	34.15	34.200000000000003	34.25	34.299999999999997	34.35	34.4	34.450000000000003	34.5	34.549999999999997	34.6	34.65	34.700000000000003	34.75	34.799999999999997	34.85	34.9	34.950000000000003	35	35.049999999999997	35.1	35.15	35.200000000000003	35.25	35.299999999999997	35.35	35.4	35.450000000000003	35.5	35.549999999999997	35.6	35.65	35.700000000000003	35.75	35.799999999999997	35.85	35.9	35.950000000000003	36	36.049999999999997	36.1	36.15	36.2000	00000000003	36.25	36.299999999999997	36.35	36.4	36.450000000000003	36.5	36.549999999999997	36.6	36.65	36.700000000000003	36.75	36.799999999999997	36.85	36.9	36.950000000000003	37	37.049999999999997	37.1	37.15	37.200000000000003	37.25	37.299999999999997	37.35	37.4	37.450000000000003	37.5	37.549999999999997	37.6	37.65	37.700000000000003	37.75	37.799999999999997	37.85	37.9	37.950000000000003	38	38.049999999999997	38.1	38.15	38.200000000000003	38.25	38.299999999999997	38.35	38.4	38.450000000000003	38.5	38.549999999999997	38.6	38.65	38.700000000000003	38.75	38.799999999999997	38.85	38.9	38.950000000000003	39	39.049999999999997	39.1	39.15	39.200000000000003	39.25	39.299999999999997	39.35	39.4	39.450000000000003	39.5	39.549999999999997	39.6	39.65	39.700000000000003	39.75	39.799999999999997	39.85	39.9	39.950000000000003	40	40.049999999999997	40.1	40.15	40.200000000000003	40.25	40.299999999999997	40.35	40.4	40.450000000000003	40.5	40.549999999999997	40.6	40.65	40.700000000000003	40.75	40.799999999999997	40.85	40.9	40.950000000000003	41	41.05	41.1	41.15	41.2	41.25	41.3	41.35	41.4	41.45	41.5	41.55	41.6	41.65	41.7	41.75	41.8	41.85	41.9	41.95	42	42.05	42.1	42.15	42.2	42.25	42.3	42.35	42.4	42.45	42.5	42.55	42.6	42.65	42.7	42.75	42.8	42.85	42.9	42.95	43	43.05	43.1	43.15	43.2	43.25	43.3	43.35	43.4	43.45	43.5	43.55	43.6	43.65	43.7	43.75	43.8	43.85	43.9	43.95	44	44.05	44.1	44.15	44.2	44.25	44.3	44.35	44.4	44.45	44.5	44.55	44.6	44.65	44.7	44.75	44.8	44.85	44.9	44.95	45	45.05	45.1	45.15	45.2	45.25	45.3	45.35	45.4	45.45	45.5	45.55	45.6	45.65	45.7	45.75	45.8	45.85	45.9	45.95	46	46.05	46.1	46.15	46.2	46.25	46.3	46.35	46.4	46.45	46.5	46.55	46.6	46.65	46.7	46.75	46.8	46.85	46.9	46.95	47	47.05	47.1	47.15	47.2	47.25	47.3	47.35	47.4	47.45	47.5	47.55	47.6	47.65	47.7	47.75	47.8	47.85	47.9	47.95	48	48.05	48.1	48.15	48.2	48.25	48.3	48.35	48.4	48.45	48.5	48.55	48.6	48.65	48.7	48.75	48.8	48.8	5	48.9	48.95	49	49.05	49.1	49.15	49.2	49.25	49.3	49.35	49.4	49.45	49.5	49.55	49.6	49.65	49.7	49.75	49.8	49.85	49.9	49.95	50	50.05	50.1	50.15	50.2	50.25	50.3	50.35	50.4	50.45	50.5	50.55	50.6	50.65	50.7	50.75	50.8	50.85	50.9	50.95	51	51.05	51.1	51.15	51.2	51.25	51.3	51.35	51.4	51.45	51.5	51.55	51.6	51.65	51.7	51.75	51.8	51.85	51.9	51.95	52	52.05	52.1	52.15	52.2	52.25	52.3	52.35	52.4	52.45	52.5	52.55	52.6	52.65	52.7	52.75	52.8	52.85	52.9	52.95	53	53.05	53.1	53.15	53.2	53.25	53.3	53.35	53.4	53.45	53.5	53.55	53.6	53.65	53.7	53.75	53.8	53.85	53.9	53.95	54	54.05	54.1	54.15	54.2	54.25	54.3	54.35	54.4	54.45	54.5	54.55	54.6	54.65	54.7	54.75	54.8	54.85	54.9	54.95	55	55.05	55.1	55.15	55.2	55.25	55.3	55.35	55.4	55.45	55.5	55.55	55.6	55.65	55.7	55.75	55.8	55.85	55.9	55.95	56	56.05	56.1	56.15	56.2	56.25	56.3	56.35	56.4	56.45	56.5	56.55	56.6	56.65	56.7	56.75	56.8	56.8	5	56.9	56.95	57	57.05	57.1	57.15	57.2	57.25	57.3	57.35	57.4	57.45	57.5	57.55	57.6	57.65	57.7	57.75	57.8	57.85	57.9	57.95	58	58.05	58.1	58.15	58.2	58.25	58.3	58.35	58.4	58.45	58.5	58.55	58.6	58.65	58.7	58.75	58.8	58.85	58.9	58.95	59	59.05	59.1	59.15	59.2	59.25	59.3	59.35	59.4	59.45	59.5	59.55	59.6	59.65	59.7	59.75	59.8	59.85	59.9	59.95	60	39	36	45	38	33	49	51	48	45	54	46	47	47	53	46	45	43	30	65	40	44	55	52	39	57	67	49	48	60	50	55	51	43	43	43	37	65	56	49	52	52	61	44	50	48	59	59	51	49	42	59	60	46	59	52	47	61	55	60	52	54	69	56	71	61	58	63	75	69	61	62	59	61	50	49	73	76	60	61	72	74	48	74	56	62	50	63	53	71	67	56	52	67	57	51	74	44	60	56	54	63	63	58	46	59	63	53	55	59	57	39	65	60	57	54	66	48	59	54	62	57	62	61	54	58	65	58	56	58	49	71	79	43	71	84	64	71	65	72	52	65	58	54	59	55	70	67	64	59	49	62	66	61	52	56	76	62	65	58	64	62	62	48	56	55	61	55	60	82	60	50	67	66	63	63	50	58	63	59	61	62	60	47	73	64	63	62	66	64	65	52	76	63	59	51	57	69	63	70	66	79	51	62	50	62	61	69	71	69	75	69	75	83	79	83	71	65	56	62	74	77	57	70	48	45	59	55	67	69	58	60	53	54	75	72	48	56	59	57	56	54	70	58	61	60	69	68	56	56	61	70	54	63	65	73	52	72	73	51	63	48	65	66	46	66	70	65	60	53	66	68	51	75	58	50	77	69	65	65	75	54	66	59	63	59	71	64	63	74	81	68	63	63	62	63	62	74	63	66	70	57	71	60	79	68	74	67	74	64	62	60	70	71	44	58	59	63	74	61	58	75	70	51	58	58	65	77	68	66	61	60	81	73	63	58	71	62	72	73	60	65	68	62	85	68	58	74	68	85	78	78	79	73	81	64	82	70	81	69	85	75	81	84	64	78	86	77	68	91	83	90	84	80	78	83	92	96	83	71	93	87	100	113	98	87	72	109	100	102	91	124	86	90	85	96	103	86	88	105	100	83	86	74	93	78	67	78	66	72	82	65	74	81	79	65	70	58	78	65	67	65	77	69	60	62	76	57	55	74	78	64	66	74	67	70	67	66	59	64	74	60	68	70	92	62	73	81	70	67	71	80	89	84	85	100	65	82	106	106	115	121	102	101	135	135	135	127	144	162	149	161	140	186	182	157	185	169	211	201	185	160	185	152	152	125	149	128	114	130	111	139	105	97	105	105	104	83	82	89	79	76	68	77	81	66	70	56	57	61	82	56	58	70	81	60	56	54	58	53	52	52	52	62	59	56	64	59	57	70	42	56	66	52	59	61	62	74	63	61	54	62	42	42	54	46	57	72	55	52	40	59	55	35	49	65	51	56	50	45	64	37	62	63	55	55	49	51	53	61	60	64	44	56	45	52	64	52	67	51	54	39	66	60	57	46	51	73	60	47	62	45	54	59	55	48	50	59	57	58	58	39	58	50	59	52	55	61	59	58	53	39	61	47	54	42	49	51	42	47	36	54	55	56	57	51	43	49	49	59	48	57	59	48	59	45	52	51	62	44	48	34	64	51	39	57	55	52	49	57	52	43	64	46	55	48	54	55	51	50	54	50	56	35	48	50	54	47	49	61	52	51	48	48	45	51	50	47	56	59	44	55	54	47	53	50	47	48	50	57	42	69	58	61	45	46	42	44	58	68	47	48	53	44	40	47	52	42	57	54	56	51	61	56	47	45	58	54	64	64	45	51	56	53	54	55	71	57	48	66	49	52	56	58	52	79	54	64	45	67	60	55	52	51	46	55	46	50	45	50	65	46	60	45	53	52	49	44	52	45	60	48	35	57	51	59	43	56	53	50	54	40	56	58	59	43	49	67	41	57	59	43	49	52	58	58	53	47	45	57	52	59	65	58	65	46	48	57	52	54	52	50	2 Theta 
Intensity

	Sample temp. ©	Diameter(nano meter)
	750	9.820033
 
	850	8.119393
 
	950	8.469314
 

Table(3): FeO temperature series at 10min and 2deg per min



Figure(3):FeO temperature series at10min and 2deg per min


temperatrue series 

Fe oxide 10 min 750 2 deg per m	20	20.05	20.100000000000001	20.149999999999999	20.2	20.25	20.3	20.350000000000001	20.399999999999999	20.45	20.5	20.55	20.6	20.65	20.7	20.75	20.8	20.85	20.9	20.95	21	21.05	21.1	21.15	21.2	21.25	21.3	21.35	21.4	21.45	21.5	21.55	21.6	21.65	21.7	21.75	21.8	21.85	21.9	21.95	22	22.05	22.1	22.15	22.2	22.25	22.3	22.35	22.4	22.45	22.5	22.55	22.6	22.65	22.7	22.75	22.8	22.85	22.9	22.95	23	23.05	23.1	23.15	23.2	23.25	23.3	23.35	23.4	23.45	23.5	23.55	23.6	23.65	23.7	23.75	23.8	23.85	23.9	23.95	24	24.05	24.1	24.15	24.2	24.25	24.3	24.35	24.4	24.45	24.5	24.5	5	24.6	24.65	24.7	24.75	24.8	24.85	24.9	24.95	25	25.05	25.1	25.15	25.2	25.25	25.3	25.35	25.4	25.45	25.5	25.55	25.6	25.65	25.7	25.75	25.8	25.85	25.9	25.95	26	26.05	26.1	26.15	26.2	26.25	26.3	26.35	26.4	26.45	26.5	26.55	26.6	26.65	26.7	26.75	26.8	26.85	26.9	26.95	27	27.05	27.1	27.15	27.2	27.25	27.3	27.35	27.4	27.45	27.5	27.55	27.6	27.65	27.7	27.75	27.8	27.85	27.9	27.95	28	28.05	28.1	28.15	28.2	28.25	28.3	28.35	28.4	28.45	28.5	28.55	28.6	28.65	28.7	28.75	28.8	28.85	28.9	28.95	29	29.05	29.1	29.15	29.2	29.25	29.3	29.35	29.4	29.45	29.5	29.55	29.6	29.65	29.7	29.75	29.8	29.85	29.9	29.95	30	30.05	30.1	30.15	30.2	30.25	30.3	30.35	30.4	30.45	30.5	30.55	30.6	30.65	30.7	30.75	30.8	30.85	30.9	30.95	31	31.05	31.1	31.15	31.2	31.25	31.3	31.35	31.4	31.45	31.5	31.55	31.6	31.65	31.7	31.75	31.8	31.85	31.9	31.95	32	32.049999999999997	32.1	32.15	32.200000000000003	32.25	32.299999999999997	32.35	32.4	32.450000000000003	32.5	32.549999999999997	32.6	32.65	32.700000000000003	32.75	32.799999999999997	32.85	32.9	32.950000000000003	33	33.049999999999997	33.1	33.15	33.200000000000003	33.25	33.299999999999997	33.35	33.4	33.450000000000003	33.5	33.549999999999997	33.6	33.65	33.700000000000003	33.75	33.799999999999997	33.85	33.9	33.950000000000003	34	34.049999999999997	34.1	34.15	34.200000000000003	34.25	34.299999999999997	34.35	34.4	34.450000000000003	34.5	34.549999999999997	34.6	34.65	34.700000000000003	34.75	34.799999999999997	34.85	34.9	34.950000000000003	35	35.049999999999997	35.1	35.15	35.200000000000003	35.25	35.299999999999997	35.35	35.4	35.450000000000003	35.5	35.549999999999997	35.6	35.65	35.700000000000003	35.75	35.799999999999997	35.85	35.9	35.950000000000003	36	36.049999999999997	36.1	36.15	36.200000000000003	36.25	36.299999999999997	36.35	36.4	36.450000000000003	36.5	36.549999999999997	36.6	36.65	36.700000000000003	36.75	36.799999999999997	36.85	36.9	36.950000000000003	37	37.049999999999997	37.1	37.15	37.200000000000003	37.25	37.299999999999997	37.35	37.4	37.450000000000003	37.5	37.549999999999997	37.6	37.65	37.700000000000003	37.75	37.799999999999997	37.85	37.9	37.950000000000003	38	38.049999999999997	38.1	38.15	38.200000000000003	38.25	38.299999999999997	38.35	38.4	38.450000000000003	38.5	38.549999999999997	38.6	38.65	38.700000000000003	38.75	38.799999999999997	38.85	38.9	38.950000000000003	39	39.049999999999997	39.1	39.15	39.200000000000003	39.25	39.299999999999997	39.35	39.4	39.450000000000003	39.5	39.549999999999997	39.6	39.65	39.700000000000003	39.75	39.799999999999997	39.85	39.9	39.950000000000003	40	40.049999999999997	40.1	40.15	40.200000000000003	40.25	40.299999999999997	40.35	40.4	40.450000000000003	40.5	40.549999999999997	40.6	40.65	40.700000000000003	40.75	40.799999999999997	40.85	40.9	40.950000000000003	41	41.05	41.1	41.15	41.2	41.25	41.3	41.35	41.4	41.45	41.5	41.55	41.6	41.65	41.7	41.75	41.8	41.85	41.9	41.95	42	42.05	42.1	42.15	42.2	42.25	42.3	42.35	42.4	42.45	42.5	42.55	42.6	42.65	42.7	42.75	42.8	42.85	42.9	42.95	43	43.05	43.1	43.15	43.2	43.25	43.3	43.35	43.4	43.45	43.5	43.55	43.6	43.65	43.7	43.75	43.8	43.85	43.9	43.95	44	44.05	44.1	44.15	44.2	44.25	44.3	44.35	44.4	44.45	44.5	44.55	44.6	44.65	44.7	44.75	44.8	44.85	44.9	44.95	45	45.05	45.1	45.15	45.2	45.25	45.3	45.35	45.4	45.45	45.5	45.55	45.6	45.65	45.7	45.75	45.8	45.85	45.9	45.95	46	46.05	46.1	46.15	46.2	46.25	46.3	46.35	46.4	46.45	46.5	46.55	46.6	46.65	46.7	46.75	46.8	46.85	46.9	46.95	47	47.05	47.1	47.15	47.2	47.25	47.3	47.35	47.4	47.45	47.5	47.55	47.6	47.65	47.7	47.75	47.8	47.85	47.9	47.95	48	48.05	48.1	48.15	48.2	48.25	48.3	48.35	48.4	48.45	48.5	48.55	48.6	48.65	48.7	48.75	48.8	48.85	48.9	48.95	49	49.05	49.1	49.15	49.2	49.25	49.3	49.35	49.4	49.45	49.5	49.55	49.6	49.65	49.7	49.75	49.8	49.85	49.9	49.95	50	364	344	360	347	375	384	400	443	455	468	457	436	405	454	389	392	381	381	377	398	348	405	375	422	400	383	368	398	388	439	409	440	468	507	464	415	374	395	377	378	428	374	379	389	410	397	374	379	407	433	409	410	390	363	432	402	405	378	391	427	387	419	369	409	355	414	409	399	372	409	432	389	411	390	393	393	393	397	384	397	378	427	387	400	413	385	410	376	379	401	423	437	386	479	533	531	496	524	458	506	441	446	441	395	405	410	409	424	408	427	422	377	399	406	390	389	393	408	407	393	391	425	384	422	438	384	401	391	389	399	408	389	379	388	426	438	401	390	404	439	410	430	442	434	493	543	702	915	1016	920	686	508	450	404	433	428	405	391	380	403	402	376	396	38	4	376	379	404	419	414	399	433	393	390	410	399	414	371	402	429	375	402	410	402	393	382	416	388	375	365	408	387	364	384	362	365	393	432	415	362	408	390	379	373	423	405	420	387	430	385	406	421	474	425	405	432	376	418	391	426	399	375	385	398	421	402	391	398	397	402	403	381	419	415	424	446	393	384	377	385	404	387	409	397	394	409	406	384	366	415	414	388	360	431	369	428	448	442	433	445	414	422	399	396	442	386	416	382	408	394	372	447	411	400	458	442	472	532	520	621	579	517	462	482	467	435	411	438	398	403	427	387	387	426	423	415	402	405	393	457	398	408	434	428	424	436	434	403	400	441	442	416	394	438	424	397	374	389	395	391	406	407	433	434	452	433	493	558	555	587	550	513	476	462	459	413	421	384	402	364	427	435	387	401	410	431	424	441	446	456	407	380	409	409	402	395	409	403	374	405	405	404	383	433	400	383	407	404	379	394	413	396	402	397	402	367	425	445	409	356	395	407	394	412	426	403	372	407	414	373	389	373	394	434	422	400	373	391	392	387	384	410	420	412	456	470	417	425	410	398	402	426	418	448	426	423	402	406	438	411	462	438	447	444	420	410	396	436	424	403	417	448	440	468	492	422	417	427	410	433	422	395	432	393	407	431	389	427	389	420	423	393	426	438	438	398	415	399	416	423	408	420	417	417	429	417	412	425	395	407	431	417	421	408	368	451	398	405	405	405	408	371	411	429	439	390	420	398	417	404	386	405	365	362	439	424	412	428	430	408	405	412	437	404	463	428	435	426	461	434	434	436	431	452	427	441	437	425	419	395	419	414	400	415	430	404	422	419	433	436	426	428	425	443	396	434	386	413	426	377	436	429	407	395	446	400	444	386	392	411	402	436	405	454	403	424	418	416	446	365	397	381	403	423	396	406	384	399	390	434	454	422	421	451	441	419	424	457	388	455	461	416	470	424	478	431	439	434	401	430	444	407	435	396	418	399	440	400	430	443	430	425	Fe oxide 	10 min 850 2 deg per m	20	20.05	20.100000000000001	20.149999999999999	20.2	20.25	20.3	20.350000000000001	20.399999999999999	20.45	20.5	20.55	20.6	20.65	20.7	20.75	20.8	20.85	20.9	20.95	21	21.05	21.1	21.15	21.2	21.25	21.3	21.35	21.4	21.45	21.5	21.55	21.6	21.65	21.7	21.75	21.8	21.85	21.9	21.95	22	22.05	22.1	22.15	22.2	22.25	22.3	22.35	22.4	22.45	22.5	22.55	22.6	22.65	22.7	22.75	22.8	22.85	22.9	22.95	23	23.05	23.1	23.15	23.2	23.25	23.3	23.35	23.4	23.45	23.5	23.55	23.6	23.65	23.7	23.75	23.8	23.85	23.9	23.95	24	24.05	24.1	24.15	24.2	24.25	24.3	24.35	24.4	24.45	24.5	24.55	24.6	24.65	24.7	24.75	24.8	24.85	24.9	24.95	25	25.05	25.1	25.15	25.2	25.25	25.3	25.35	25.4	25.45	25.5	25.55	25.6	25.65	25.7	25.75	25.8	25.85	25.9	25.95	26	26.05	26.1	26.15	26.2	26.25	26.3	26.35	26.4	26.45	26.5	26.55	26.6	26.65	26.7	26.75	26.8	26.85	26.9	26.95	27	27.05	27.1	27.15	27.2	27.25	27.3	27.35	27.4	27.45	27.5	27.55	27.6	27.65	27.7	27.75	27.8	27.85	27.9	27.95	28	28.05	28.1	28.15	28.2	28.25	28.3	28.35	28.4	28.45	28.5	28.55	28.6	28.65	28.7	28.75	28.8	28.85	28.9	28.95	29	29.05	29.1	29.15	29.2	29.25	29.3	29.35	29.4	29.45	29.5	29.55	29.6	29.65	29.7	29.75	29.8	29.85	29.9	29.95	30	30.05	30.1	30.15	30.2	30.25	30.3	30.35	30.4	30.45	30.5	30.55	30.6	30.65	30.7	30.75	30.8	30.85	30.9	30.95	31	31.05	31.1	31.15	31.2	31.25	31.3	31.35	31.4	31.45	31.5	31.55	31.6	31.65	31.7	31.75	31.8	31.85	31.9	31.95	32	32.049999999999997	32.1	32.15	32.200000000000003	32.25	32.299999999999997	32.35	32.4	32.450000000000003	32.5	32.549999999999997	32.6	32.65	32.700000000000003	32.75	32.799999999999997	32.85	32.9	32.950000000000003	33	33.049999999999997	33.1	33.15	33.200000000000003	33.25	33.299999999999997	33.35	33.4	33.450000000000003	33.5	33.549999999999997	33.6	33.65	33.700000000000003	33.75	33.799999999999997	33.85	33.9	33.950000000000003	34	34.049999999999997	34.1	34.15	34.200000000000003	34.25	34.299999999999997	34.35	34.4	34.450000000000003	34.5	34.549999999999997	34.6	34.65	34.700000000000003	34.75	34.799999999999997	34.85	34.9	34.950000000000003	35	35.049999999999997	35.1	35.15	35.200000000000003	35.25	35.299999999999997	35.35	35.4	35.450000000000003	35.5	35.549999999999997	35.6	35.65	35.700000000000003	35.75	35.799999999999997	35.85	35.9	35.950000000000003	36	36.049999999999997	36.1	36.15	36.200000000000003	36.25	36.299999999999997	36.35	36.4	36.450000000000003	36.5	36.549999999999997	36.6	36.65	36.700000000000003	36.75	36.799999999999997	36.85	36.9	36.950000000000003	37	37.049999999999997	37.1	37.15	37.200000000000003	37.25	37.299999999999997	37.35	37.4	37.450000000000003	37.5	37.549999999999997	37.6	37.65	37.700000000000003	37.75	37.799999999999997	37.85	37.9	37.950000000000003	38	38.049999999999997	38.1	38.15	38.200000000000003	38.25	38.299999999999997	38.35	38.4	38.450000000000003	38.5	38.549999999999997	38.6	38.65	38.700000000000003	38.75	38.799999999999997	38.85	38.9	38.950000000000003	39	39.049999999999997	39.1	39.15	39.200000000000003	39.25	39.299999999999997	39.35	39.4	39.450000000000003	39.5	39.549999999999997	39.6	39.65	39.700000000000003	39.75	39.799999999	999997	39.85	39.9	39.950000000000003	40	40.049999999999997	40.1	40.15	40.200000000000003	40.25	40.299999999999997	40.35	40.4	40.450000000000003	40.5	40.549999999999997	40.6	40.65	40.700000000000003	40.75	40.799999999999997	40.85	40.9	40.950000000000003	41	41.05	41.1	41.15	41.2	41.25	41.3	41.35	41.4	41.45	41.5	41.55	41.6	41.65	41.7	41.75	41.8	41.85	41.9	41.95	42	42.05	42.1	42.15	42.2	42.25	42.3	42.35	42.4	42.45	42.5	42.55	42.6	42.65	42.7	42.75	42.8	42.85	42.9	42.95	43	43.05	43.1	43.15	43.2	43.25	43.3	43.35	43.4	43.45	43.5	43.55	43.6	43.65	43.7	43.75	43.8	43.85	43.9	43.95	44	44.05	44.1	44.15	44.2	44.25	44.3	44.35	44.4	44.45	44.5	44.55	44.6	44.65	44.7	44.75	44.8	44.85	44.9	44.95	45	45.05	45.1	45.15	45.2	45.25	45.3	45.35	45.4	45.45	45.5	45.55	45.6	45.65	45.7	45.75	45.8	45.85	45.9	45.95	46	46.05	46.1	46.15	46.2	46.25	46.3	46.35	46.4	46.45	46.5	46.55	46.6	46.65	46.7	46.75	46.8	46.85	46.9	46.95	47	47.05	47.1	47.15	47.2	47.25	47.3	47.35	47.4	47.45	47.5	47.55	47.6	47.65	47.7	47.75	47.8	47.85	47.9	47.95	48	48.05	48.1	48.15	48.2	48.25	48.3	48.35	48.4	48.45	48.5	48.55	48.6	48.65	48.7	48.75	48.8	48.85	48.9	48.95	49	49.05	49.1	49.15	49.2	49.25	49.3	49.35	49.4	49.45	49.5	49.55	49.6	49.65	49.7	49.75	49.8	49.85	49.9	49.95	50	294	308	303	280	285	323	332	324	293	350	340	380	376	339	354	365	323	326	279	326	318	338	307	326	305	321	336	307	296	372	321	275	342	368	428	402	392	364	343	305	292	308	346	287	310	324	331	312	329	341	320	305	331	334	345	297	354	343	359	364	339	318	329	320	325	338	324	331	335	349	355	344	363	361	307	319	317	335	333	316	316	305	317	330	341	322	284	343	332	331	350	357	338	335	336	386	397	403	434	454	407	402	364	359	334	338	347	301	328	316	308	294	305	334	313	283	298	342	325	324	349	329	318	357	331	301	337	320	341	336	320	301	317	358	330	314	341	338	320	337	324	369	320	332	331	360	393	442	542	717	712	691	565	378	348	346	324	343	349	321	337	335	336	357	326	288	316	330	359	328	331	324	316	311	350	301	370	308	331	318	340	338	359	329	314	358	329	345	331	329	326	338	342	335	299	324	362	317	320	304	328	322	316	291	299	342	345	353	342	309	325	312	336	357	386	404	387	338	354	323	364	331	336	334	352	321	318	328	353	321	338	346	329	349	348	339	313	340	319	377	361	308	358	341	310	331	332	309	351	312	353	328	338	348	349	341	335	347	360	339	380	375	338	323	351	336	348	346	355	352	316	351	358	375	372	350	415	390	412	499	542	531	481	420	376	359	380	369	316	348	384	337	322	366	337	340	339	352	313	357	330	362	347	356	363	367	369	339	373	385	336	339	351	343	355	345	350	354	348	329	322	339	358	356	335	380	363	393	455	470	479	457	431	422	380	350	328	364	366	357	356	355	370	373	359	349	360	363	364	392	368	373	345	333	384	334	359	338	361	338	322	338	318	373	352	379	341	371	346	350	339	333	350	349	343	372	341	312	338	361	354	341	335	340	368	332	356	340	353	348	325	324	320	333	361	352	372	331	324	351	360	341	340	413	379	375	404	383	369	404	370	342	339	379	350	368	387	346	345	338	364	345	367	382	379	349	386	370	349	358	337	370	384	353	385	371	417	392	375	374	381	366	333	387	358	372	367	339	365	354	387	341	356	349	364	371	348	396	358	351	410	360	324	385	370	385	355	360	354	383	356	363	400	353	361	387	349	366	381	329	342	368	320	347	333	358	336	369	351	397	362	338	352	358	385	343	337	332	365	351	346	343	350	388	353	354	400	335	381	378	377	367	380	391	371	357	354	362	394	349	377	334	354	368	339	372	344	372	333	370	378	356	356	354	394	360	352	384	361	348	374	350	387	360	373	360	371	381	365	327	383	367	366	363	366	340	365	340	350	355	358	389	363	345	406	354	372	363	349	353	378	377	355	386	354	349	354	381	380	347	388	368	388	356	382	400	404	364	373	350	397	349	367	418	346	384	376	387	356	403	374	Fe oxide 10 min 950 2 deg per min	20	20.05	20.100000000000001	20.149999999999999	20.2	20.25	20.3	20.350000000000001	20.399999999999999	20.45	20.5	20.55	20.6	20.65	20.7	20.75	20.8	20.85	20.9	20.95	21	21.05	21.1	21.15	21.2	21.25	21.3	21.35	21.4	21.45	21.5	21.55	21.6	21.65	21.7	21.75	21.8	21.85	21.9	21.95	22	22.05	22.1	22.15	22.2	22.25	22.3	22.35	22.4	22.45	22.5	22.55	22.6	22.65	22.7	22.75	22.8	22.85	22.9	22.95	23	23.05	23.1	23.15	23.2	23.25	23.3	23.35	23.4	23.45	23.5	23.55	23.6	23.65	23.7	23.75	23.8	23.85	23.9	23.95	24	24.05	24.1	24.15	24.2	24.25	24.3	24.35	24.4	24.45	24.5	24.55	24.6	24.65	24.7	24.75	24.8	24.85	24.9	24.95	25	25.05	25.1	25.15	25.2	25.2	5	25.3	25.35	25.4	25.45	25.5	25.55	25.6	25.65	25.7	25.75	25.8	25.85	25.9	25.95	26	26.05	26.1	26.15	26.2	26.25	26.3	26.35	26.4	26.45	26.5	26.55	26.6	26.65	26.7	26.75	26.8	26.85	26.9	26.95	27	27.05	27.1	27.15	27.2	27.25	27.3	27.35	27.4	27.45	27.5	27.55	27.6	27.65	27.7	27.75	27.8	27.85	27.9	27.95	28	28.05	28.1	28.15	28.2	28.25	28.3	28.35	28.4	28.45	28.5	28.55	28.6	28.65	28.7	28.75	28.8	28.85	28.9	28.95	29	29.05	29.1	29.15	29.2	29.25	29.3	29.35	29.4	29.45	29.5	29.55	29.6	29.65	29.7	29.75	29.8	29.85	29.9	29.95	30	30.05	30.1	30.15	30.2	30.25	30.3	30.35	30.4	30.45	30.5	30.55	30.6	30.65	30.7	30.75	30.8	30.85	30.9	30.95	31	31.05	31.1	31.15	31.2	31.25	31.3	31.35	31.4	31.45	31.5	31.55	31.6	31.65	31.7	31.75	31.8	31.85	31.9	31.95	32	32.049999999999997	32.1	32.15	32.200000000000003	32.25	32.299999999999997	32.35	32.4	32.450000000000003	32.5	32.549999999999997	32.6	32.65	32.700000000000003	32.75	32.799999999999997	32.85	32.9	32.950000000000003	33	33.049999999999997	33.1	33.15	33.200000000000003	33.25	33.299999999999997	33.35	33.4	33.450000000000003	33.5	33.549999999999997	33.6	33.65	33.700000000000003	33.75	33.799999999999997	33.85	33.9	33.950000000000003	34	34.049999999999997	34.1	34.15	34.200000000000003	34.25	34.299999999999997	34.35	34.4	34.450000000000003	34.5	34.549999999999997	34.6	34.65	34.700000000000003	34.75	34.799999999999997	34.85	34.9	34.950000000000003	35	35.049999999999997	35.1	35.15	35.200000000000003	35.25	35.299999999999997	35.35	35.4	35.450000000000003	35.5	35.549999999999997	35.6	35.65	35.700000000000003	35.75	35.799999999999997	35.85	35.9	35.950000000000003	36	36.049999999999997	36.1	36.15	36.200000000000003	36.25	36.299999999999997	36.35	36.4	36.450000000000003	36.5	36.549999999999997	36.6	36.65	36.700000000000003	36.75	36.799999999999997	36.85	36.9	36.950000000000003	37	37.049999999999997	37.1	37.15	37.200000000000003	37.25	37.299999999999997	37.35	37.4	37.450000000000003	37.5	37.549999999999997	37.6	37.65	37.700000000000003	37.75	37.799999999999997	37.85	37.9	37.950000000000003	38	38.049999999999997	38.1	38.15	38.200000000000003	38.25	38.299999999999997	38.35	38.4	38.450000000000003	38.5	38.549999999999997	38.6	38.65	38.700000000000003	38.75	38.799999999999997	38.85	38.9	38.950000000000003	39	39.049999999999997	39.1	39.15	39.200000000000003	39.25	39.299999999999997	39.35	39.4	39.450000000000003	39.5	39.549999999999997	39.6	39.65	39.700000000000003	39.75	39.799999999999997	39.85	39.9	39.950000000000003	40	40.049999999999997	40.1	40.15	40.200000000000003	40.25	40.299999999999997	40.35	40.4	40.450000000000003	40.5	40.549999999999997	40.6	40.65	40.700000000000003	40.75	40.799999999999997	40.85	40.9	40.950000000000003	41	41.05	41.1	41.15	41.2	41.25	41.3	41.35	41.4	41.45	41.5	41.55	41.6	41.65	41.7	41.75	41.8	41.85	41.9	41.95	42	42.05	42.1	42.15	42.2	42.25	42.3	42.35	42.4	42.45	42.5	42.55	42.6	42.65	42.7	42.75	42.8	42.85	42.9	42.95	43	43.05	43.1	43.15	43.2	43.25	43.3	43.35	43.4	43.45	43.5	43.55	43.6	43.65	43.7	43.75	43.8	43.85	43.9	43.95	44	44.05	44.1	44.15	44.2	44.25	44.3	44.35	44.4	44.45	44.5	44.55	44.6	44.65	44.7	44.75	44.8	44.85	44.9	44.95	45	45.05	45.1	45.15	45.2	45.25	45.3	45.35	45.4	45.45	45.5	45.55	45.6	45.65	45.7	45.75	45.8	45.85	45.9	45.95	46	46.05	46.1	46.15	46.2	46.25	46.3	46.35	46.4	46.45	46.5	46.55	46.6	46.65	46.7	46.75	46.8	46.85	46.9	46.95	47	47.05	47.1	47.15	47.2	47.25	47.3	47.35	47.4	47.45	47.5	47.55	47.6	47.65	47.7	47.75	47.8	47.85	47.9	47.95	48	48.05	48.1	48.15	48.2	48.25	48.3	48.35	48.4	48.45	48.5	48.55	48.6	48.65	48.7	48.75	48.8	48.85	48.9	48.95	49	49.05	49.1	49.15	49.2	49.25	49.3	49.35	49.4	49.45	49.5	49.55	49.6	49.65	49.7	49.75	49.8	49.85	49.9	49.95	50	214	193	219	205	193	197	224	188	219	201	250	218	261	266	269	264	240	267	197	248	246	211	244	216	225	202	249	221	230	219	229	214	241	228	269	251	251	289	281	223	235	221	228	215	232	197	253	235	199	263	210	219	245	227	225	257	201	252	236	240	258	223	206	205	236	222	208	226	217	216	215	241	253	200	224	225	233	230	206	228	223	213	230	218	207	242	211	240	235	233	230	241	213	235	260	264	258	255	259	291	329	330	304	276	270	270	256	213	259	235	240	227	243	235	216	246	243	238	238	195	233	226	254	221	251	229	226	242	241	238	248	263	264	225	253	247	228	246	243	236	228	266	234	219	252	244	239	265	288	317	384	515	603	584	433	321	244	266	226	252	231	241	245	225	257	240	223	227	241	242	258	230	233	253	237	254	238	215	231	230	219	259	231	214	206	215	234	256	238	217	255	248	240	224	250	246	232	248	243	225	249	231	231	234	247	239	232	270	242	250	223	249	284	229	250	258	283	238	266	270	266	272	242	241	270	236	242	250	240	235	253	250	244	248	237	238	243	238	232	259	234	265	263	221	244	249	235	251	256	241	236	277	235	231	240	250	279	247	275	260	230	291	258	258	248	245	247	239	243	261	235	242	254	252	252	242	273	249	272	264	294	372	423	425	413	353	277	281	251	264	274	265	262	265	263	255	241	254	239	251	235	235	254	265	243	258	279	269	279	258	270	240	282	261	261	245	270	253	232	231	259	241	266	252	241	258	263	256	278	301	310	364	374	375	370	296	266	261	277	269	241	250	244	276	254	271	280	258	267	260	296	272	291	265	288	252	280	257	237	261	252	240	250	240	265	267	246	252	230	248	258	266	236	236	272	258	248	249	249	273	243	237	263	250	265	259	246	255	272	242	265	231	230	247	255	261	265	244	250	231	240	269	251	255	254	262	276	282	307	317	302	276	292	271	251	274	260	263	255	268	246	280	274	286	271	289	280	260	301	272	276	292	235	286	274	279	274	279	277	278	304	276	287	301	262	296	281	251	249	267	282	253	247	287	253	295	273	252	255	277	253	257	248	238	243	301	307	292	269	281	285	254	281	288	251	247	264	307	240	247	257	277	253	220	253	266	258	252	284	278	295	259	291	244	277	235	269	258	240	273	258	264	283	287	278	272	291	235	302	249	261	290	271	273	277	275	279	292	299	313	266	273	290	300	265	269	270	310	278	276	245	231	271	278	283	277	277	267	268	280	295	293	266	268	270	266	251	246	258	264	297	281	272	246	272	265	290	287	294	285	280	290	275	260	259	257	285	272	273	291	251	294	268	285	276	253	290	280	267	283	277	295	276	284	289	296	295	271	301	318	280	285	276	280	313	286	254	274	296	300	268	2 Theta


Intensity





	Sample time (min)	Diameter(nano meter)
	5	11.45671
 
	10	9.820033
 

Table(4):FeO time series at 750 c and 2deg per min




Figure(4):FeO time series at750 C and 2deg per min


TIME SERIES FOR FeO

Fe oxide 5 min 750 2 deg per min	20	20.05	20.100000000000001	20.149999999999999	20.2	20.25	20.3	20.350000000000001	20.399999999999999	20.45	20.5	20.55	20.6	20.65	20.7	20.75	20.8	20.85	20.9	20.95	21	21.05	21.1	21.15	21.2	21.25	21.3	21.35	21.4	21.45	21.5	21.55	21.6	21.65	21.7	21.75	21.8	21.85	21.9	21.95	22	22.05	22.1	22.15	22.2	22.25	22.3	22.35	22.4	22.45	22.5	22.55	22.6	22.65	22.7	22.75	22.8	22.85	22.9	22.95	23	23.05	23.1	23.15	23.2	23.25	23.3	23.35	23.4	23.45	23.5	23.55	23.6	23.65	23.7	23.75	23.8	23.85	23.9	23.95	24	24.05	24.1	24.15	24.2	24.25	24.3	24.35	24.4	24.45	24.5	24.55	24.6	24.65	24.7	24.75	24.8	24.85	24.9	24.95	25	25.05	25.1	25.15	25.2	25.25	25.3	25.35	25.4	25.45	25.5	25.55	25.6	25.65	25.7	25.75	25.8	25.85	25.9	25.95	26	26.05	26.1	26.15	26.2	26.25	26.3	26.35	26.4	26.45	26.5	26.55	26.6	26.65	26.7	26.75	26.8	26.85	26.9	26.95	27	27.05	27.1	27.15	27.2	27.25	27.3	27.35	27.4	27.45	27.5	27.55	27.6	27.65	27.7	27.75	27.8	27.85	27.9	27.95	28	28.05	28.1	28.15	28.2	28.25	28.3	28.35	28.4	28.45	28.5	28.55	28.6	28.65	28.7	28.75	28.8	28.85	28.9	28.95	29	29.05	29.1	29.15	29.2	29.25	29.3	29.35	29.4	29.45	29.5	29.55	29.6	29.65	29.7	29.75	29.8	29.85	29.9	29	.95	30	30.05	30.1	30.15	30.2	30.25	30.3	30.35	30.4	30.45	30.5	30.55	30.6	30.65	30.7	30.75	30.8	30.85	30.9	30.95	31	31.05	31.1	31.15	31.2	31.25	31.3	31.35	31.4	31.45	31.5	31.55	31.6	31.65	31.7	31.75	31.8	31.85	31.9	31.95	32	32.049999999999997	32.1	32.15	32.200000000000003	32.25	32.299999999999997	32.35	32.4	32.450000000000003	32.5	32.549999999999997	32.6	32.65	32.700000000000003	32.75	32.799999999999997	32.85	32.9	32.950000000000003	33	33.049999999999997	33.1	33.15	33.200000000000003	33.25	33.299999999999997	33.35	33.4	33.450000000000003	33.5	33.549999999999997	33.6	33.65	33.700000000000003	33.75	33.799999999999997	33.85	33.9	33.950000000000003	34	34.049999999999997	34.1	34.15	34.200000000000003	34.25	34.299999999999997	34.35	34.4	34.450000000000003	34.5	34.549999999999997	34.6	34.65	34.700000000000003	34.75	34.799999999999997	34.85	34.9	34.950000000000003	35	35.049999999999997	35.1	35.15	35.200000000000003	35.25	35.299999999999997	35.35	35.4	35.450000000000003	35.5	35.549999999999997	35.6	35.65	35.700000000000003	35.75	35.799999999999997	35.85	35.9	35.950000000000003	36	36.049999999999997	36.1	36.15	36.200000000000003	36.25	36.299999999999997	36.35	36.4	36.450000000000003	36.5	36.549999999999997	36.6	36.65	36.700000000000003	36.75	36.799999999999997	36.85	36.9	36.950000000000003	37	37.049999999999997	37.1	37.15	37.200000000000003	37.25	37.299999999999997	37.35	37.4	37.450000000000003	37.5	37.549999999999997	37.6	37.65	37.700000000000003	37.75	37.799999999999997	37.85	37.9	37.950000000000003	38	38.049999999999997	38.1	38.15	38.200000000000003	38.25	38.299999999999997	38.35	38.4	38.450000000000003	38.5	38.549999999999997	38.6	38.65	38.700000000000003	38.75	38.799999999999997	38.85	38.9	38.950000000000003	39	39.049999999999997	39.1	39.15	39.200000000000003	39.25	39.299999999999997	39.35	39.4	39.450000000000003	39.5	39.549999999	999997	39.6	39.65	39.700000000000003	39.75	39.799999999999997	39.85	39.9	39.950000000000003	40	40.049999999999997	40.1	40.15	40.200000000000003	40.25	40.299999999999997	40.35	40.4	40.450000000000003	40.5	40.549999999999997	40.6	40.65	40.700000000000003	40.75	40.799999999999997	40.85	40.9	40.950000000000003	41	41.05	41.1	41.15	41.2	41.25	41.3	41.35	41.4	41.45	41.5	41.55	41.6	41.65	41.7	41.75	41.8	41.85	41.9	41.95	42	42.05	42.1	42.15	42.2	42.25	42.3	42.35	42.4	42.45	42.5	42.55	42.6	42.65	42.7	42.75	42.8	42.85	42.9	42.95	43	43.05	43.1	43.15	43.2	43.25	43.3	43.35	43.4	43.45	43.5	43.55	43.6	43.65	43.7	43.75	43.8	43.85	43.9	43.95	44	44.05	44.1	44.15	44.2	44.25	44.3	44.35	44.4	44.45	44.5	44.55	44.6	44.65	44.7	44.75	44.8	44.85	44.9	44.95	45	45.05	45.1	45.15	45.2	45.25	45.3	45.35	45.4	45.45	45.5	45.55	45.6	45.65	45.7	45.75	45.8	45.85	45.9	45.95	46	46.05	46.1	46.15	46.2	46.25	46.3	46.35	46.4	46.45	46.5	46.55	46.6	46.65	46.7	46.75	46.8	46.85	46.9	46.95	47	47.05	47.1	47.15	47.2	47.25	47.3	47.3	5	47.4	47.45	47.5	47.55	47.6	47.65	47.7	47.75	47.8	47.85	47.9	47.95	48	48.05	48.1	48.15	48.2	48.25	48.3	48.35	48.4	48.45	48.5	48.55	48.6	48.65	48.7	48.75	48.8	48.85	48.9	48.95	49	49.05	49.1	49.15	49.2	49.25	49.3	49.35	49.4	49.45	49.5	49.55	49.6	49.65	49.7	49.75	49.8	49.85	49.9	49.95	50	50.05	50.1	50.15	50.2	50.25	50.3	50.35	50.4	50.45	50.5	50.55	50.6	50.65	50.7	50.75	50.8	50.85	50.9	50.95	51	51.05	51.1	51.15	51.2	51.25	51.3	51.35	51.4	51.45	51.5	51.55	51.6	51.65	51.7	51.75	51.8	51.85	51.9	51.95	52	52.05	52.1	52.15	52.2	52.25	52.3	52.35	52.4	52.45	52.5	52.55	52.6	52.65	52.7	52.75	52.8	52.85	52.9	52.95	53	53.05	53.1	53.15	53.2	53.25	53.3	53.35	53.4	53.45	53.5	53.55	53.6	53.65	53.7	53.75	53.8	53.85	53.9	53.95	54	54.05	54.1	54.15	54.2	54.25	54.3	54.35	54.4	54.45	54.5	54.55	54.6	54.65	54.7	54.75	54.8	54.85	54.9	54.95	55	55.05	55.1	55.15	55.2	55.25	55.3	55.3	5	55.4	55.45	55.5	55.55	55.6	55.65	55.7	55.75	55.8	55.85	55.9	55.95	56	56.05	56.1	56.15	56.2	56.25	56.3	56.35	56.4	56.45	56.5	56.55	56.6	56.65	56.7	56.75	56.8	56.85	56.9	56.95	57	57.05	57.1	57.15	57.2	57.25	57.3	57.35	57.4	57.45	57.5	57.55	57.6	57.65	57.7	57.75	57.8	57.85	57.9	57.95	58	58.05	58.1	58.15	58.2	58.25	58.3	58.35	58.4	58.45	58.5	58.55	58.6	58.65	58.7	58.75	58.8	58.85	58.9	58.95	59	59.05	59.1	59.15	59.2	59.25	59.3	59.35	59.4	59.45	59.5	59.55	59.6	59.65	59.7	59.75	59.8	59.85	59.9	59.95	60	334	347	361	410	321	404	405	411	472	395	465	428	430	423	356	384	369	393	372	372	381	353	389	385	414	374	368	385	351	388	396	428	516	582	509	448	341	406	410	385	394	390	380	394	374	406	399	383	426	400	391	391	410	403	395	412	406	410	406	407	398	381	419	401	390	365	408	388	390	391	398	381	412	407	409	383	410	383	401	404	441	374	387	367	373	404	411	416	418	388	379	421	401	446	468	548	520	479	457	473	432	438	451	414	416	389	405	404	465	427	435	395	357	411	415	395	411	363	395	422	408	402	411	420	437	400	395	414	397	437	407	395	364	400	402	429	387	407	407	390	391	420	417	405	460	506	688	967	1073	1030	732	532	461	436	395	449	427	392	402	382	410	401	434	399	408	389	372	391	380	395	400	383	401	422	440	364	403	393	402	400	369	417	373	386	407	358	393	401	378	358	368	412	412	413	388	377	399	419	417	409	400	418	398	446	362	380	416	401	416	433	384	423	446	425	434	441	407	427	408	407	404	421	396	423	411	451	400	418	418	409	386	428	411	417	424	448	446	433	418	407	375	421	392	432	435	413	446	426	404	432	456	405	402	409	400	420	424	441	450	453	435	413	403	433	412	420	446	402	427	429	417	429	425	473	455	476	560	546	558	559	555	524	472	475	477	442	462	435	412	440	398	433	414	429	427	401	424	418	428	432	421	372	432	443	446	434	402	426	454	415	454	434	401	430	447	401	412	361	419	394	413	429	456	443	488	456	493	527	572	582	537	506	488	385	459	452	397	431	417	450	422	428	436	426	427	440	471	457	419	461	437	421	411	426	430	413	402	434	393	448	420	427	412	397	445	434	415	409	408	429	414	388	432	441	368	430	393	421	397	413	414	439	412	420	386	454	418	407	378	404	451	410	395	410	438	411	385	417	410	413	427	405	420	441	509	509	424	426	402	429	403	429	400	424	409	422	389	440	414	398	425	438	455	454	450	448	449	429	459	467	453	463	494	470	486	452	486	472	439	455	415	425	442	421	419	439	446	448	469	399	401	446	433	463	400	394	398	438	398	448	449	399	443	421	440	468	433	454	417	394	421	435	427	425	406	434	435	397	461	431	436	389	455	423	434	413	416	400	412	487	398	428	436	459	429	448	435	394	430	408	452	436	470	454	473	452	474	439	442	429	431	430	465	430	456	455	450	426	452	404	446	410	437	439	448	479	441	422	375	471	461	441	426	421	397	453	455	416	437	418	472	411	433	455	403	437	417	440	417	452	445	404	453	434	435	428	407	459	447	458	428	435	426	433	479	441	421	414	424	446	444	445	431	410	454	436	431	429	448	454	467	409	472	482	485	477	448	472	444	455	421	432	439	439	438	456	428	492	436	461	470	Fe oxide 10 min 750 2 deg per m	20	20.05	20.100000000000001	20.149999999999999	20.2	20.25	20.3	20.350000000000001	20.399999999999999	20.45	20.5	20.55	20.6	20.65	20.7	20.75	20.8	20.85	20.9	20.95	21	21.05	21.1	21.15	21.2	21.25	21.3	21.35	21.4	21.45	21.5	21.55	21.6	21.65	21.7	21.75	21.8	21.85	21.9	21.95	22	22.05	22.1	22.15	22.2	22.25	22.3	22.35	22.4	22.45	22.5	22.55	22.6	22.65	22.7	22.75	22.8	22.85	22.9	22.95	23	23.05	23.1	23.15	23.2	23.25	23.3	23.35	23.4	23.45	23.5	23.55	23.6	23.65	23.7	23.75	23.8	23.85	23.9	23.95	24	24.05	24.1	24.15	24.2	24.25	24.3	24.35	24.4	24.45	24.5	24.55	24.6	24.65	24.7	24.75	24.8	24.85	24.9	24.95	25	25.05	25.1	25.15	25.2	25.25	25.3	25.35	25.4	25.45	25.5	25.55	25.6	25.65	25.7	25.75	25.8	25.85	25.9	25.95	26	26.05	26.1	26.15	26.2	26.25	26.3	26.35	26.4	26.45	26.5	26.55	26.6	26.65	26.7	26.75	26.8	26.85	26.9	26.95	27	27.05	27.1	27.15	27.2	27.25	27.3	27.35	27.4	27.45	27.5	27.55	27.6	27.65	27.7	27.75	27.8	27.85	27.9	27.95	28	28.05	28.1	28.15	28.2	28.25	28.3	28.35	28.4	28.45	28.5	28.55	28.6	28.65	28.7	28.75	28.8	28.85	28.9	28.95	29	29.05	29.1	29.15	29.2	29.25	29.3	29.35	29.4	29.45	29.5	29.55	29.6	29.65	29.7	29.75	29.8	29.85	29.9	29.95	30	30.05	30.1	30.15	30.2	30.25	30.3	30.35	30.4	30.45	30.5	30.55	30.6	30.65	30.7	30.75	30.8	30.85	30.9	30.95	31	31.05	31.1	31.15	31.2	31.25	31.3	31.35	31.4	31.45	31.5	31.55	31.6	31.65	31.7	31.75	31.8	31.85	31.9	31.95	32	32.049999999999997	32.1	32.15	32.200000000000003	32.25	32.299999999999997	32.35	32.4	32.450000000000003	32.5	32.549999999999997	32.6	32.65	32.700000000000003	32.75	32.799999999999997	32.85	32.9	32.950000000000003	33	33.0499999999	99997	33.1	33.15	33.200000000000003	33.25	33.299999999999997	33.35	33.4	33.450000000000003	33.5	33.549999999999997	33.6	33.65	33.700000000000003	33.75	33.799999999999997	33.85	33.9	33.950000000000003	34	34.049999999999997	34.1	34.15	34.200000000000003	34.25	34.299999999999997	34.35	34.4	34.450000000000003	34.5	34.549999999999997	34.6	34.65	34.700000000000003	34.75	34.799999999999997	34.85	34.9	34.950000000000003	35	35.049999999999997	35.1	35.15	35.200000000000003	35.25	35.299999999999997	35.35	35.4	35.450000000000003	35.5	35.549999999999997	35.6	35.65	35.700000000000003	35.75	35.799999999999997	35.85	35.9	35.950000000000003	36	36.049999999999997	36.1	36.15	36.200000000000003	36.25	36.299999999999997	36.35	36.4	36.450000000000003	36.5	36.549999999999997	36.6	36.65	36.700000000000003	36.75	36.799999999999997	36.85	36.9	36.950000000000003	37	37.049999999999997	37.1	37.15	37.200000000000003	37.25	37.299999999999997	37.35	37.4	37.450000000000003	37.5	37.549999999999997	37.6	37.65	37.700000000000003	37.75	37.799999999999997	37.85	37.9	37.950000000000003	38	38.049999999999997	38.1	38.15	38.200000000000003	38.25	38.299999999999997	38.35	38.4	38.450000000000003	38.5	38.549999999999997	38.6	38.65	38.700000000000003	38.75	38.799999999999997	38.85	38.9	38.950000000000003	39	39.049999999999997	39.1	39.15	39.200000000000003	39.25	39.299999999999997	39.35	39.4	39.450000000000003	39.5	39.549999999999997	39.6	39.65	39.700000000000003	39.75	39.799999999999997	39.85	39.9	39.950000000000003	40	40.049999999999997	40.1	40.15	40.200000000000003	40.25	40.299999999999997	40.35	40.4	40.450000000000003	40.5	40.549999999999997	40.6	40.65	40.700000000000003	40.75	40.799999999999997	40.85	40.9	40.950000000000003	41	41.05	41.1	41.15	41.2	41.25	41.3	41.35	41.4	41.45	41.5	41.55	41.6	41.65	41.7	41.75	41.8	41.85	41.9	41.95	42	42.05	42.1	42.15	42.2	42.25	42.3	42.35	42.4	42.45	42.5	42.55	42.6	42.65	42.7	42.75	42.8	42.85	42.9	42.95	43	43.05	43.1	43.15	43.2	43.25	43.3	43.35	43.4	43.45	43.5	43.55	43.6	43.65	43.7	43.75	43.8	43.85	43.9	43.95	44	44.05	44.1	44.15	44.2	44.25	44.3	44.35	44.4	44.45	44.5	44.55	44.6	44.65	44.7	44.75	44.8	44.85	44.9	44.95	45	45.05	45.1	45.15	45.2	45.25	45.3	45.35	45.4	45.45	45.5	45.55	45.6	45.65	45.7	45.75	45.8	45.85	45.9	45.95	46	46.05	46.1	46.15	46.2	46.25	46.3	46.35	46.4	46.45	46.5	46.55	46.6	46.65	46.7	46.75	46.8	46.85	46.9	46.95	47	47.05	47.1	47.15	47.2	47.25	47.3	47.35	47.4	47.45	47.5	47.55	47.6	47.65	47.7	47.75	47.8	47.85	47.9	47.95	48	48.05	48.1	48.15	48.2	48.25	48.3	48.35	48.4	48.45	48.5	48.55	48.6	48.65	48.7	48.75	48.8	48.85	48.9	48.95	49	49.05	49.1	49.15	49.2	49.25	49.3	49.35	49.4	49.45	49.5	49.55	49.6	49.65	49.7	49.75	49.8	49.85	49.9	49.95	50	50.05	50.1	50.15	50.2	50.25	50.3	50.35	50.4	50.45	50.5	50.55	50.6	50.65	50.7	50.75	50.8	50.85	50.9	50.95	51	51.05	51.1	51.15	51.2	51.25	51.3	51.35	51.4	51.45	51.5	51.55	51.6	51.65	51.7	51.75	51.8	51.85	51.9	51.95	52	52.05	52.1	52.15	52.2	52.25	52.3	52.35	52.4	52.45	52.5	52.55	52.6	52.65	52.7	52.75	52.8	52.85	52.9	52.95	53	53.05	53.1	53.15	53.2	53.25	53.3	53.35	53.4	53.45	53.5	53.55	53.6	53.65	53.7	53.75	53.8	53.85	53.9	53.95	54	54.05	54.1	54.15	54.2	54.25	54.3	54.35	54.4	54.45	54.5	54.55	54.6	54.65	54.7	54.75	54.8	54.85	54.9	54.95	55	55.05	55.1	55.15	55.2	55.25	55.3	55.35	55.4	55.45	55.5	55.55	55.6	55.65	55.7	55.75	55.8	55.85	55.9	55.95	56	56.05	56.1	56.15	56.2	56.25	56.3	56.35	56.4	56.45	56.5	56.55	56.6	56.65	56.7	56.75	56.8	56.85	56.9	56.95	57	57.05	57.1	57.15	57.2	57.25	57.3	57.35	57.4	57.45	57.5	57.55	57.6	57.65	57.7	57.75	57.8	57.85	57.9	57.95	58	58.05	58.1	58.15	58.2	58.25	58.3	58.35	58.4	58.45	58.5	58.55	58.6	58.65	58.7	58.75	58.8	58.85	58.9	58.95	59	59.05	59.1	59.15	59.2	59.25	59.3	59.35	59.4	59.45	59.5	59.55	59.6	59.65	59.7	59.75	59.8	59.85	59.9	59.95	60	364	344	360	347	375	384	400	443	455	468	457	436	405	454	389	392	381	381	377	398	348	405	375	422	400	383	368	398	388	439	409	440	468	507	464	415	374	395	377	378	428	374	379	389	410	397	374	379	407	433	409	410	390	363	432	402	405	378	391	427	387	419	369	409	355	414	409	399	372	409	432	389	411	390	393	393	393	397	384	397	378	427	387	400	413	385	410	376	379	401	423	437	386	479	533	531	496	524	458	506	441	446	441	395	405	410	409	424	408	427	422	377	399	406	390	389	393	408	407	393	391	425	384	422	438	384	401	391	389	399	408	389	379	388	426	438	401	390	404	439	410	430	442	434	493	543	702	915	1016	920	686	508	450	404	433	428	405	391	380	403	402	376	396	384	376	379	404	419	414	399	433	393	390	410	399	414	371	402	429	375	402	410	402	393	382	416	388	375	365	408	387	364	384	362	365	393	432	415	362	408	390	379	373	423	405	420	387	430	385	406	421	474	425	405	432	376	418	391	426	399	375	385	398	421	402	391	398	397	402	403	381	419	415	424	446	393	384	377	385	404	387	409	397	394	409	406	384	366	415	414	388	360	431	369	428	448	442	433	445	414	422	399	396	442	386	416	382	408	394	372	447	411	400	458	442	472	532	520	621	579	517	462	482	467	435	411	438	398	403	427	387	387	426	423	415	402	405	393	457	398	408	434	428	424	436	434	403	400	441	442	416	394	438	424	397	374	389	395	391	406	407	433	434	452	433	493	558	555	587	550	513	476	462	459	413	421	384	402	364	427	435	387	401	410	431	424	441	446	456	407	380	409	409	402	395	409	403	374	405	405	404	383	433	400	383	407	404	379	394	413	396	402	397	402	367	425	445	409	356	395	407	394	412	426	403	372	407	414	373	389	373	394	434	422	400	373	391	392	387	384	410	420	412	456	470	417	425	410	398	402	426	418	448	426	423	402	406	438	411	462	438	447	444	420	410	396	436	424	403	417	448	440	468	492	422	417	427	410	433	422	395	432	393	407	431	389	427	389	420	423	393	426	438	438	398	415	399	416	423	408	420	417	417	429	417	412	425	395	407	431	417	421	408	368	451	398	405	405	405	408	371	411	429	439	390	420	398	417	404	386	405	365	362	439	424	412	428	430	408	405	412	437	404	463	428	435	426	461	434	434	436	431	452	427	441	437	425	419	395	419	414	400	415	430	404	422	419	433	436	426	428	425	443	396	434	386	413	426	377	436	429	407	395	446	400	444	386	392	411	402	436	405	454	403	424	418	416	446	365	397	381	403	423	396	406	384	399	390	434	454	422	421	451	441	419	424	457	388	455	461	416	470	424	478	431	439	434	401	430	444	407	435	396	418	399	440	400	430	443	430	425	2 Theta


Intensity 




Errors and Difficulties 
The accuracy of the balance while weighting the samples. 
It have been discovered the all ceramic crucible’s were used shows high percentage of error.
There was some human error, which make us do more trials for each sample.
 Long time to do XRD test for each sample



Conclusion 
The preparation of metal oxide in this project was synthesized by hydrothermal method. 
There was a theoretical loss that was calculated. 
Samples were tested in XRD, then Miniflex draw the result to find later its diameter. The results of our samples in general for MgO were from (1.2 – 3.7) nm ,  As for the FeO the results were (8.1-11.4)nm .
Finally our goal have been achieved, as the assumption that was made become real , Nano size exist in the samples .



Recommendation

1- There should be X-Ray Diffraction device in An-Najah University
2- Safety tools should be available , with better quality due to dealing with high temperature .
3- special crucible material should available , it result in the product quality .




The end 



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