An-Najah National University Faculty of Graduate Studies Utilization of Waste Tires in the Production of Non- Structural Portland Cement Concrete By Saleem Mohammed Saleem Shtayeh Supervisor Dr. Osama Abaza Submitted in Partial Fulfillment of the Requirements for the Degree of Master in Transportation Engineering, Faculty of Graduate Studies, at An-Najah National University, Nablus, Palestine 2007 iii DEDICATION To the owners of the glowing hearts and burning vigor.………………. To those who sacrificed their money, souls and blood for their faith..... To those who faced the devil of evil and the devil of craving…………. To my tender mother, honored father, dear my wife, my daughter, brothers and sisters. To all of them, I dedicate this work iv ACKNOWLEDGMENT Thank God for the blessing granted to us………………….................... I feel obliged to extend my sincere thanks to my instructors at An- Najah National University, who were helpful and brace. They were really that burning candles to illuminate our path. And special thanks to Dr. Osama Abaza who saved no effort in supporting me to complete this work in spite of the difficult circumstances. I also would like to thank the discussion committee instructors Dr. Khaled Al-Sahili and Dr. Sami Hijjawi who had a great effect in achieving the benefit. Finally many heartfelt thanks go to my dear brothers, sisters and friends who helped me in this modest work. v TABLE OF CONTENTS Number Content Page Number LIST OF TABLES vii LIST OF FIGURES viii LIST OF APPENDICES x ABSTRACT xi CHAPTER ONE: INTRODUCTION 1 1.1 Background 2 1.2 Problem Statement 4 1.3 Goals and Objectives 6 CHAPTER TWO: LIBRARY SEARCH 8 2.1 Background 9 2.2 Tire Manufacturing 9 2.2.1 Manufacture of crumb tire 10 2.2.1.1 Mechanical Grinding 12 2.2.1.2 Cryogenics 14 2.3 Civil Engineering Applications of Recycled Rubber from Scrap Tires 15 2.3.1 Sub-grade Insulation for Roads 16 2.3.2 Sub-grade Fill and Embankments 16 2.3.3 Backfill for Walls and Bridge Abutments 17 2.3.4 Landfills 17 2.3.5 Other Uses 18 2.4 Studies and Research 20 2.5 Fresh concrete Properties Containing Scrap-rubber Tires 25 2.5.1 Slump 25 2.5.2 Air Content 26 2.5.3 Unit Weight 26 2.5.4 Hardened Properties 26 2.5.5 Shrinkage 30 2.5.6 Toughness and Impact Resistance 31 2.5.7 Freezing and thawing resistance 33 CHAPTER THREE: METHODOLOGY 36 3.1 Introduction 37 3.2 Work Procedure 37 3.2.1 Materials 37 3.2.2 Raw Material tests 38 3.2.3 Plain Portland cement concrete mixes 38 3.2.4 Crumb Portland cement concrete mixes 40 3.3 Tests on PCC 43 vi 3.4 Thermal and sound insulation testing 44 CHAPTER FOUR: EXPERIMENTAL TESTS RESULTS 48 4.1 Introduction 49 4.2 Materials testing results 49 4.3 Concrete Compressive strength and slump tests results 52 4.4 Density test results 53 4.5 Water Absorption test results 54 4.6 Abrasion resistance of concrete test results 55 4.7 Modulus of elasticity test results 56 4.8 Noise insulation test results 57 4.9 Thermal insulation test results 58 CHAPTER FIVE: ANALYSIS OF RESULTS 59 5.1 Introduction 60 5.2 Compressive strength 60 5.3 Density 65 5.4 Water absorption 67 5.5 Slump (consistency) 69 5.6 Abrasion 69 5.7 Modulus of elasticity 71 5.8 Noise insulation 72 5.9 Thermal insulation 76 5.10 Particles distribution 77 CHAPTER SIX: CONCLUSIONS AND RECOMMENDATIONS 79 6.1 Introduction 80 6.2 Conclusions 80 6.3 Recommendations 81 REFERENCES 83 APPENDICES 90 ب الملخص vii LIST OF TABLES Table Number Page Number Table 1.1 Weights of scrap tires for different classes of vehicles in the West Bank 5 Table 2.1 Typical materials used in manufacturing tire 12 Table 3.1 Concrete mix design by weight of mix ingredients (kg/m3 of PCC) 39 Table 3.2 Mix ingredients (kg/0.01m3 of PCC) 39 Table 3.3 Grade B-150 of PCC for batch mix 41 Table 3.4 Grade B-200 of PCC for batch mix 41 Table 3.5 Grade B-250 of PCC for batch mix 42 Table 3.6 Grade B-300 of PCC for batch mix 42 Table 3.7 Grade B-450 of PCC for batch mix 43 Table 4.1 Materials tests results 50 Table 4.2 Concrete compressive strength test results 52 Table 4.3 Density test results 53 Table 4.4 Concrete water absorption test results 54 Table 4.5 Concrete abrasion test results 55 Table 4.6 Modulus of elasticity test results 56 Table 4.7 Noise insulation test results 57 Table 4.8 Thermal insulation test results 58 viii LIST OF FIGURES Figure Number Contents Page Number Figure 1.1 Used tires waste in an open area 3 Figure 1.2 Waste tire dump on fire 4 Figure 1.3 Weights chart of scrap tires 5 Figure 1.4 Weight fraction Chart of total weight of scrap tires 5 Figure 2.1 Flow Chart Summarizing Tire Manufacturing Process 11 Figure 2.2 Typical Shredding Waste Tire Machine 14 Figure 2.3 Shredded scrap tires used as road base 17 Figure 3.1 Concrete mold (15x15x15cm Dimension) 44 Figure 3.2 Wooden box face with two opening one for source and the other for measuring (40x40x100cm Dimension) 45 Figure 3.3 Wooden box back (the other face) with one opening for measuring. 46 Figure 3.4 Specimen location (at the middle of the wooden box) with frame dimension 15x15x15 cm 46 Figure 4.1 Particle size distribution 51 Figure 5.1 Percent replacement by crumb waste tires versus compressive strength for PCC-150 60 Figure 5.2 Percent replacement by crumb waste tires versus compressive strength for PCC-150+200 62 Figure 5.3 Percent replacement by crumb waste tires versus compressive strength for various PCC categories 63 Figure 5.4 Compressive strength of Portland cement concrete for various percentages of replacement of crumbed waste tires 64 Figure 5.5 Percent replacement by crumb waste tires versus density for PCC-150 65 Figure 5.6 Percent replacement by crumb waste tires versus density for various categories of concrete 66 Figure 5.7 Percent replacement by crumb waste tires versus Water Absorption for PCC-150 67 Figure 5.8 Percent replacement by crumb waste tires versus Water Absorption for various categories of concrete 68 Figure 5.9 Percent replacement by crumb waste tires versus slump for various PCC categories 69 ix Figure 5.10 Percent replacement by crumb waste tires versus abrasion for PCC-150 70 Figure 5.11 Percent replacement by crumb waste tires versus abrasion for various PCC categories 71 Figure 5.12 Stress versus strain for PCC-300 71 Figure 5.13 Percent replacement by crumb waste tires versus elasticity for various PCC categories 72 Figure 5.14 Percent replacement by crumb waste tires versus reduction of noise at low level for various PCC categories 73 Figure 5.15 Percent replacement by crumb waste tires versus reduction of noise at high level for various PCC categories 74 Figure 5.16 Percent replacement by crumb waste tires versus average reduction of noise at low and high level 75 Figure 5.17 Percent replacement by crumb waste tires versus temperature reduction for various PCC categories 76 Figure 5.18 Percent replacement by crumb waste tires versus average temperature reduction for various PCC categories 77 Figure 5.19 Particles distribution 78 x LIST OF APPENDICES Appendix Contents Page Number Appendix A Compressive strength test results tables 91 Appendix B Stress – strain figures 105 xi Utilization of Waste Tires in the Production of Non-Structural Portland Cement Concrete By Saleem Mohammed Saleem Shtayeh Supervisor Dr. Osama A. Abaza Abstract This thesis, generally, aims to explore the potential utilization of waste crumb tires in various Portland Cement Concrete categories for the production of non-structural Portland cement concrete to study the structural behavior of concrete, and to help partially solving environmental problem produced from disposing waste tires. Raw materials of coarse and fine aggregate used in this thesis were tested, fine aggregate (sand) was replaced using volumetric method by waste crumb tires with 0, 25, 50, 75, and 100% replacements for the various PCC categories of B-150, 200, 250, 300, and B-450 kg/cm2. Several tests were made on fresh and hardened concrete, like compressive strength, slump, water absorption, density, modulus of elasticity, noise and thermal insulation tests, and abrasion resistance, Compressive strength, density, and modulus of elasticity decreased as the percent replacement by waste crumb tires increased; water absorption initially decreased and started to increase after an increasing in the percent of replacement, slump showed no significant change. Abrasion resistance, noise and thermal insulation increased as the percent replacement increased. xii Finally it is recommended to use waste crumb tires for non-structural Portland cement concrete, such as floor rips, partitions, back stone concrete, concrete blocks, and other non-structural uses. Key words: Portland cement concrete, waste crumb tire, physical properties, utilization, non-structural concrete. CHAPTER ONE INTRODUCTION 2 CHAPTER ONE INTRODUCTION 1.1 Background Modifications of construction materials have an important bearing on the building sector. Several attempts have been therefore made in the building material industry to put to use waste material products, e.g., worn-out tires, into useful and cost effective items. Success in this regard will contribute to the reduction of waste material dumping problems by utilizing the waste materials as raw material for other products. The waste problem considered as one of the most crucial problems facing the world as a source of the environmental pollution. It is contributing as a direct form in pollution that includes the negative effects on the health by increasing the diseases, diseases vector, percentage of mortality and lowering the standard of living. The waste usually defined as the all remains things resulted from production, transfer and uses processes, and in general all transmitted things and resources that the owner or the producer wants to dispose or must dispose to prevent the risk on the health of the human and save the environment in general. During last recent years, many improvements in West Bank have occurred in all parts of life such as social, industrial, economical etc. Like all countries in the world, this will lead to generate new ways of living and 3 increase the human requirements, and will also increase types and quantities of the waste in the West Bank, without any active processes to provide solution to this problem. One of the important types of remains is waste tires which have been classified as a part of municipal solid waste (MSW), resulted from the increase of vehicle ownership and traffic volume within the Palestinian territories. This eventually will increase consumption of tires over time. Current practices show that residents throw it randomly in different places such as valleys, road sides, open areas, and waste dumpsites in improper ways taking the means of open fire, and without consideration of risk on human health and environment. Figures 1.1 and 1.2 show some of the forms of dumping and wrong practices for waste tires. Figure 1.1: Used tires waste in an open area 4 Figure 1.2: Waste tire dump on fire 1.2 Problem Statement In presenting the properties of tires, it can be seen that tire is a rubber article with a complex structure, in which rubber represents approximately (85%) of the weight of car or truck tires (DiChristina 1994). The average tire life is 50,000 km, after which it must be replaced (DiChristina 1994). In the assessment of the size of this environmental problem, the weights of scrap tires generating in the West Bank is given in Table 1.1 and Figs.1.3, and 1.4 (Israeli Central Bureau of Statistics, 2005). 5 Table (1.1): Weights of scrap tires for different classes of vehicles in the West Bank Type of Vehicles Weight of tires (Ton/Year) Private car 2500 Light truck up to 10 ton 2000 Heavy trucks and buses 2300 Agriculture and heavy equipment 700 Other vehicles 500 Total 8000 Source: Israeli Central Bureau of statistics, 2005 Figure 1.3: Weights chart of scrap tires Figure 1.4: Weight fraction chart of total weight of scrap tires Waste rubber tires cause serious environmental problems all over the world. One of the potential means of utilizing the waste tires is to process this waste material for the protection of the environment and society. It is 2500 2000 2300 700 500 private cars Heavy trucks up 10 ton Heavy trucks and buses Agriculture and heavy equipment Other vehicles 31% 25% 29% 9% 6% Private cars Heavy trucks up 10 ton Heavy trucks and buses Agriculture and heavy equipment Other vehicles 6 suggested to use this waste tires as an additive in Portland cement concrete (PCC) mixes for non-structural applications, which would partially help in solving this problem. 1.3 Goals and Objectives This research aims to help in assisting partially the environmental issue resulted from disposing waste vehicle tires. The objective of this research is to investigate the utilization of rubber tires in the form of shredded tires (crumbs) in PCC for non-structural concrete through investigating its impact on the physical characteristics of PCC as compressive strength, workability, water absorption (porosity), noise insulation, thermal insulation, and abrasion. Detailed review of different studies and researches about utilizing waste tires in several applications is presented in Chapter Two. This chapter includes background about waste tire as an environmental problem, civil engineering application of recycled rubber from scrap tires, properties of concrete containing scrap tires, tires manufacturing, typical chemical composition and crumb manufacturing. Chapter Three presents the methodology of utilizing rubber waste tires by using this waste as a constituent of the PCC mixes by partial or full replacement of fine aggregate (sand), and the experimental tests used in this thesis to identify the materials and the tests on the concrete mixes. 7 Experimental tests results are presented in Chapter Four. Chapter Five illustrated the analysis of the results. Chapter Six concludes the work done in this thesis, it emphasizes on the importance of studying the utilization of waste tires in the production of these kinds of concrete mixes, and the recommendations of the future working is also presented in this chapter. 8 CHAPTER TWO LIBRARY SEARCH 9 CHAPTER TWO LIBRARY SEARCH 2.1 Background Solid waste management is one of the major environmental concerns in the world. Each year thousands of tires are added to stockpiles, landfills, and illegal dumps across the West Bank and Gaza Strip, which causes extensive environmental and hazardous problems. Waste tires stockpiles are dangerous not only due to potential environmental threat, but also from fire hazards and creating a breeding grounds for rats, mice, vermin’s and mosquitoes (Naik and Singh 1991, Singh 1993). Over the years, disposal of tires has become one of the serious problems for the environment. Land-filling is becoming unacceptable for waste tires because of the rapid depletion of available sites for waste disposal. In France, which produces over 10 million scrap-tires per year will have a dwindling supply of landfills starting from July 2002; due to a new law that forbids any new landfill in the country. Used tires are required to be shredded before land-filling. Innovative solutions to meet the challenge of tire disposal problem have long been in development. 2.2 Tire Manufacturing The tire manufacturing process includes the manufacture of rubber and placing additives in the rubber. It also includes the coating of fabrics for 10 the radial belts and bias plies and integrating them into the rubber. Rayon, nylon, and now more commonly polyester in addition to building wire bead stock, make up the structural components of tires. The fabric with rubber, the bead stock with rubber, and the rubber tread is combined on a drum by layering (the tread is put on last). There can be as many as 40 layers of fabric and steel bead wire on a truck tire. Once the layers are put on, the tire stock is put into a mold over an inflatable steam heated tube. The tube is inflated and the mold is closed. The tire is heated and cured and the excess rubber extrudes out of weep holes in the mold. Curing times and temperatures vary widely between manufacturers and tire compositions. Typical curing times are around 20 minutes with temperatures around 160°F. The curing is the vulcanization takes place (CIWMB 1994). Figure 2.1 shows a flow chart of the process of manufacturing and Table 2.1 gives the typical materials used in manufacturing tires. 2.2.1 Manufacture of Crumb Rubber Crumb rubber is made by a combination or application of several size reduction technologies. These technologies may be divided into two major processing categories, mechanical grinding and cryogenic reduction. 11 synthetic rubber natural rubber carbon black plasticizers accelerators nylon fabric rayon fabric sheet processer tread extruder bead wire builder tire building ply layering curing mixer compound rubber polyester fabric brass coated steel wire steel wire finished tire Source: (CIWMB 1994) Figure 2.1: Flow Chart Summarizing Tire Manufacturing Process 12 Table 2.1 Typical materials used in manufacturing tire 1. Synthetic rubber 2. Natural rubber 3. Sulfur and sulfur compounds 4. Phenolic resin 5. Oil (i) Aromatic (ii) Naphthenic (iii) Paraffinic 6. Fabric (i) Polyester (ii) Nylon 7. Petroleum waxes 8. Pigments (i) Zinc oxide (ii) Titanium dioxide 9. Carbon black 10. Fatty acids 11. Inert materials 12. Steel wires Source: (Siddique et al 2004) 2.2.1.1 Mechanical Grinding Mechanical grinding is the most commonly used process. The method consists of mechanically breaking down the rubber into small particles using a variety of grinding techniques, such as cracker mills, granulators, etc. The steel components are removed by a magnetic separator (sieve shakers and conventional separators, such as centrifugal, air classification, density etc. are also used). The fiber components are separated by air classifiers or other separation equipment. These systems are well established and can produce crumb rubber (varying particle size, grades, 13 quality etc.) at relatively low cost. The system is easy to maintain and requires few people to operate and service. Replacement parts are generally easy to obtain and install. The other important advantage of mechanical grinding relates to the shape and physical properties of the crumb rubber particles. The shape and surface texture of the crumb rubber particles are relatively rounded and smooth, and are able to form molecular cross-links with virgin rubber material. The rubber particles are broken down under high shear stress. Since the tire compound consists of a carbon-sulfur cross- linked matrix, the grinding process causes 'de-linking' of the material. The resulting 'de-linked' material is more viscous compared to virgin rubber and is a unique characteristic of mechanically ground crumb rubber. For applications involving compounding with virgin rubber or plastic, crumb rubber provides some advantageous attributes to the viscoelastic compound. The crumb rubber particles do not cause a deterioration of tensile strength at low to moderate loading (Blumenthal 1998). The main disadvantage is related to cost. Figure 2.2 shows a typical waste tire machine. 14 Figure 2.2: Typical Shredding Waste Tire Machine 2.2.1.2 Cryogenics The cryogenic process consists of freezing the shredded rubber at an extremely low temperature (far below the glass transition temperature of the compound). The frozen rubber compound is then easily shattered into small particles. The fiber and steel are removed in the same fashion as in mechanical grinding. The advantages of the system are cleaner and faster operation resulting in the production of fine mesh size. The most significant disadvantage is the slightly higher cost due to the added cost of cooling (liquid nitrogen, etc.) (Blumenthal 1998). 15 2.3 Civil Engineering Applications of Recycled Rubber from Scrap Tires Scrap tire chips and their granular counterpart, crumb rubber, have been successfully used in a number of civil engineering applications. Tire chips consist of tire pieces that are roughly shredded into 2.5 to 30 cm lengths. They often contain fabric and steel belts that are exposed at the cut edge of the tire chip. Tire chips have been researched extensively as lightweight fill for embankments and retaining walls (Tweedie et al. 1998, Bosscher et al. 1997, Masad et al. 1996, Upton and Machan 1993, Humphrey and Manion 1992), but have also been used as drainage layers for roads and in septic tank leach fields (Humphrey 1999). According to Humphrey (1999), some of the advantageous properties of tire chips in civil engineering applications include low material density, high bulk permeability, high thermal insulation, high durability, and high bulk compressibility. In many cases, scrap tire chips may also represent the least expensive alternative to other fill materials. Crumb rubber is a finely ground tire rubber from which the fabric and steel belts have been removed. It has a granular texture and ranges in size from very fine powder to sand-sized particles. Crumb rubber has been successfully used as an alternative aggregate source in both asphalt concrete and PCC. This waste material has been used in several engineering structures like highway Base-courses, embankments, etc. No local experience have been 16 recorded any utilization or management of this waste material, on the contrary, several cases of fatal and hazardous conditions occur on daily bases as a result of ignorance and bad handling of this waste material. It is important to note that the generation of this material on daily basis locally and world wide is beyond tolerated level, which makes it an urgent and a standing issue to deal with. 2.3.1 Subgrade Insulation for Roads Excess water is released when subgrade soils thaw in the spring. Placing a 15 to 30 cm thick tire shred layer under the road cab prevents the subgrade soils from freezing in the first place. In addition, the high permeability of tire shreds allows water to drain from beneath the roads, preventing damage to road surfaces (ASTM D6270-98). Figure 2.3 shows a typical layout of shredded tires for highway construction. (Tires manufacture's Association, 2003). 2.3.2 Subgrade Fill and Embankments Tire shreds can be used to construct embankments on weak, compressible foundation soils. Tire shreds are viable in this application due to their light weight. For most projects, using tire shreds as a lightweight fill material is significantly a cheaper alternative. (Tires manufacture's Association, 2003). 17 Figure 2.3: Shredded scrap tires used as road base 2.3.3 Backfill for Walls and Bridge Abutments Tire shreds can be useful as backfill for walls and bridge abutments. The weight of the tire shreds reduces horizontal pressures and allows for construction of thinner, less expensive walls. Tire shreds can also reduce problems with water and frost build-up behind walls because tire shreds are free draining and provide good thermal insulation. Recent research has demonstrated the benefits of using tire shreds in backfill for walls and bridge abutments. (Tires manufacture's Association, 2003). 2.3.4 Landfills Landfill construction and operation is a growing market application for tire shreds. Scrap tire shreds can replace other construction materials that would have to be purchased. Scrap tires may be used as a lightweight 18 backfill in gas venting systems, in leachate collection systems, and in operational liners. They may also be used in landfill capping and closures, and as a material for daily cover. (Tires manufacture's Association, 2003). 2.3.5 Other Uses Fattuhi and Clark (1996) have suggested that rubcrete could possibly be used in the following areas: 1. Where vibration damping is needed, such as in foundation pad for rotating machinery and in railway stations, 2. For trench filling and pipe bedding, pile heads, and paving slabs, and 3. For resistance to impact or blast is required such as in railway buffers, jersey barriers (a protective concrete barrier used as a highway divider and a means of preventing access to a prohibited area) and bunkers. Rubcrete, because of its light unit weight (density ranges from 900 to 1600 kg/m3) may also be suitable for architectural applications such as: (1) Nailing concrete, (2) False facades, (3) Stone backing and (4) Interior construction. Topcu and Avcular (1997) have suggested that rubber-concrete may be used in highway construction as: (1) Shock absorber in sound barriers, (2) Sound boaster (which controls the sound effectively), and (3) in buildings as an earthquake shock-wave absorber. However, research is needed before definite recommendations can be made. 19 Al-Akhras and Smadi (2002) studied the properties of tire-rubber ash (TRA) mortar. Tire rubber chips were obtained and burned at a controlled temperature of 850 Cº for 72 hours. The residue of tire-rubber chips (ash) was collected. TRA was utilized as partial replacement of sand in five percentages ranging from 0% to 10% with an increment of 2.5% by weight of sand. Based on the test results, they concluded that: as the TRA content increased, the workability of the fresh mortar decreased. This behavior is due to the increase in the cementitiouse materials in the mortar mix, due particularly to the large surface area of the added TRA. In addition both initial and final setting time increased with the increase in TRA content. The initial setting time increased from 145 min for the control paste mix to 220 min for 10% TRA paste mix. The final setting time increased from 270 min for control paste mix to 390 min for 10% TRA paste mix. Further more the TRA specimens showed higher compressive strengths at various curing periods up to 90 days compared with those of the control specimens. Also, the tensile and flexural strengths of the TRA mortar specimens were higher than those of the control specimens. Pierce and Blackwell (2003) in their paper highlighted the use of crumb rubber in flowable fill. In their investigation, they replaced sand with crumb rubber to produce flowable fill. Experimental results indicated that crumb rubber can be successfully used to produce a lightweight (1.2–1.6 g/cm3) flowable fill with excavatable 28-day compressive strengths ranging from 0.02 to 0.09 MPa. Based on their investigation, they concluded that a crumb rubber-based flowable fill can be used in a substantial number of 20 construction applications, such as bridge abutment fills, trench fills and foundation fills. The following are also some examples on using scrap tires: - Playground surface material. - Gravel substitute. - Drainage around building foundations and building foundation insulation. - Erosion control/rainwater runoff barriers (whole tires). - Wetlands/marsh establishment (whole tires). - Crash barriers around race tracks (whole tires). - Boat bumpers at marinas (whole tires). - Artificial reefs (whole tires). 2.4 Studies and Research The use of rubber waste shredded tires was studied in the past by many researchers. Chunk rubber from recycled tires was used as a road construction material; the feasibility of using large rubber chunks from shredded tires as aggregates in cold-mixes for road construction was investigated (Hossain 1995). The research was directed toward development of a chunk rubber 21 asphalt concrete mix design for low volume road construction using local aggregate, shredded tire rubber chunks and a cationic emulsion. A set of mixes using different combinations of chunk rubber content, emulsion content and fly ash content were tested. Based on the Marshall Stability results, some of these mixes appeared to be suitable as binder courses or stabilized drainable bases for low volume roads. In asphalt rubber pavement for the purpose of producing asphalt rubber pavements, old tires are shredded to make crumbs of rubber about the size of coarse sand. This rubber is then mixed with asphalt and cement. The resulting mix is then blended with aggregates such as sand or crushed gravel using conventional methods to produce the mixture of paving material. A research in construction of a test embankment using a sand–tire shred mixture as fill material was made (Sungmin et al. 2005). Use of tire shreds in construction projects, such as highway embankments, is becoming an accepted way of beneficially recycling scrap tires. Sungmin indicated that mixtures of tire shreds and sand are viable materials for embankment construction. Another research work was made for the determination of the optimum conditions for tire rubber in asphalt concrete (Ahmet et al. 2004). Tire rubber waste recycling in self-compacting concrete, the rubber waste tire was used in this kind of concrete and the mechanical and micro structural behavior were investigated in the study. 22 A systematic experimental study was performed recently for improving strength and toughness of Rubber Modified Concrete (RMC) (Xi et al. 2003). Two types of rubber particles of different sizes (large and small) were used to study the size effect on mechanical properties of RMC. Result of tension test, fatigue test, and ultrasound velocity test showed that the RMC has higher energy dissipation capacities than regular concrete, that is, the RMC has high toughness and high ductility. As a result, there is an increase in the toughness and ductility. The failure modes of the RMC indicate that the RMC samples can withhold very large deformation and still keep their integrity. Waste tire steel beads were also used in PCC. The experimental results indicate that although the compressive strength is reduced when steel beads are used, the toughness of the material greatly increases. Moreover, the workability of the mixtures fabricated was not significantly affected (Christos and Matthew 2006) In the study of the development of waste tire modified concrete, two types of waste tire configurations were evaluated (Guoqiang et al. 2004). One was in the form of chips, or particles and the other was in the form of fibers. Conclusions showed that fibers performed better than chips do. Although thinner fibers perform better than thicker fibers do, the effect was not very significant. Steel belt wires in waste tires had a positive effect on increasing the strength of rubberized concrete. Truck tires performed better than car tires did. 23 Another research was done using Chopped Worn-Out Tires in production of light weight concrete masonry units (Al-Hadithi et al. 1999). This research, generally aimed at defining the possibility of using chopped worn-out tires to produce lightweight concrete building units. Many experimental mixtures were made with different percentages of chopped worn-out tires after identifying the importance of produced characteristics of the mixtures. For producing lightweight Chopped worn-out tires concrete mixes, many trials were adopted in selecting the required mixes. The methodology of aggregate replacement was to substitute a certain volume of aggregate by the same volume of Chopped worn-out tires, but with different partial replacement ratios (PRR'S) for the sand and the gravel. For production and testing Chopped worn-out tires in Hollow- Concrete blocks units with a new suggested geometry, in addition to the conventional units, to enhance the structural properties of walls and the other properties which are provided by using Chopped worn-out tires, five short walls were built from fine-block using both Chopped worn-out tires (concrete and mortar) mixes with their corresponding plain mixes (without Chopped worn-out tires). Also two short walls were built from traditional Hollow-Concrete block with two holes using plain mixes (without chopped worn-out tires). 24 These walls were tested to study the structural behavior of such walls. All the mixes used Ordinary Portland Cement. The sand was a washed and dried natural river sand with a size range of (0.15-4.75mm), with bulk specific gravity 2.6. The gravel was washed and dried natural gravel with a size range of 1.18 to 9.5 mm, with specific gravity of 2.7. The Chopped worn-out tires used in this work had a maximum size of 6.35mm and a specific gravity of 0.95. The dry constituents were initially mixed for 1.0 minute with Chopped worn-out tires mixes, the Chopped worn-out tires were then incorporated into the dry mix through a dispenser, and the mixing continued for another 1.0 minute to allow uniform distribution of the Chopped worn-out tires in the mixture. After adding the water, the constituents were then mixed for a further 2.0 minutes to produce a homogeneous mixture. Different specimens were prepared and a number of tests were made, the tests included compressive strength, axially load capacity of walls and prisms, measurement of longitudinal and traverse strains were made on both faces of walls using mechanical extensometers with high sensitivity. The main conclusions from this investigations were incorporating Chopped worn-out tires into the mortar and concrete mixes as a partial replacement of aggregate reduced its unit weight, compressive strength and flexural strength and increased its thermal insulation significantly, the Chopped worn-out tires concrete masonry wall had numerous benefits especially in the reduction of the dead loads, improving the thermal insulation and 25 provided a satisfactory structural function, the absorption of the Chopped worn-out tires concrete units was within the range of ACI 531-83 requirements for the corresponding lightweight masonry unit, the performance of fin-blocks was superior as compared with that of conventional blocks, and cracks occurred simultaneously in masonry units and mortar, these cracks which developed in a masonry wall before failure were visible to the naked eye. 2.5 Fresh Concrete Properties Containing Scrap-rubber Tires 2.5.1 Slump Raghvan et al. (1998) reported that mortars incorporating rubber shreds achieved workability (defined as the ease with which mortar/concrete can be mixed, transported and placed) comparable to or better than a control mortar without rubber particles. Khatib and Bayomy (1999) investigated the workability of rubber concrete and reported that there was a decrease in slump with increase in rubber content as a percentage of total aggregate volume. They further noted that at rubber contents of 40%, slump was almost zero and concrete was not workable manually. It was also observed that mixtures made with fine crumb rubber were more workable than those with coarse tire chips or a combination of tire chips and crumb rubber. 26 2.5.2 Air Content Fedro et al. (1996) have reported higher air content in rubber concrete mixtures than control mixtures even without the use of air-entraining admixture (AEA). Similar observations were also made by Khatib and Bayomy (1999). This may be due to the non-polar nature of rubber particles and their tendency to entrap air in their out surfaces. Also when rubber was added to a concrete mixture, it might attract air as it had the tendency to repel water, and then air might adhere to the rubber particles. Therefore, increasing the rubber content results in higher air contents in rubber concrete mixtures, there by, decreasing the unit weight of the mixtures. 2.5.3 Unit Weight Because of low specific gravity of rubber particles, unit weight of mixtures containing rubber decreases with the increase in the percentage of rubber content. Moreover, increase in rubber content increased the air content, which in turn reduced the unit weight of the mixtures. The decrease in unit weight of rubber concrete was negligible when rubber content is lower than 10–20% of the total aggregate volume (Khatib and Bayomy 1999). 2.5.4 Hardened Properties Several authors (Ali et al. 1993, Rostami et al. 1993, Eldin and Senouci 1993, Topcu 1995) reported the compressive strength results of rubberized concrete. Results of various studies indicated that the size, proportions and 27 surface texture of rubber particles noticeably affected compressive strength of rubber concrete mixtures. Eldin and Senouci (1993) reported that concrete mixtures with tire chips and crumb rubber aggregates exhibited lower compressive and splitting tensile strengths than regular PCC. There was approximately 85% reduction in compressive strength and 50% reduction in splitting tensile strength when coarse aggregate was fully replaced by coarse crumb rubber chips. However, a reduction of about 65% in compressive strength and up to 50% in splitting tensile strength was observed when fine aggregate was fully replaced by fine crumb rubber. Both of these mixtures demonstrated a ductile failure and had the ability to absorb a large amount of energy under compressive and tensile loads Khatib and Bayomy (1999). Topcu (1995) also showed that the addition of coarse rubber-chips in concrete lowered the compressive strength more than the addition of fine crumb rubber. However, results reported by Ali et al (1993) and Fattuhi and Clark (1996) indicated the opposite trend. Studies have indicated that if the rubber particles have rougher surface or given a pretreatment, then better and improved bonding may develop with the surrounding matrix, and, therefore, that may result in higher compressive strength. Pretreatments may vary from washing rubber particles with water to acid etching, plasma pretreatment and various coupling agents (Naik and Singh 1991). 28 In acid pretreatment, rubber particles are soaked in an alkaline solution (NaOH) for 5 minutes and then rinsed with water. This treatment enhances the strength of concrete containing rubber particles through a microscopic (a very small) increase in the surface texture of the rubber particles. Eldin and Senouci (1993) soaked and thoroughly washed rubber aggregates with water to remove contaminants, while Rostami et al. (1993) used water, water and carbon tetrachloride solvent, and water and a latex admixture cleaner. Results showed that concrete containing water washed rubber particles achieved about 16% higher compressive strength than concrete containing untreated rubber aggregates, whereas this improvement in compressive strength was 57% when rubber aggregates treated with carbon tetrachloride were used. Segre and Joekes (2000) worked on the use of tire rubber particles as addition to cement paste. In their work, the surface of powdered tire rubber (particles of maximum size 35 mesh, 500 μm) was modified to increase its adhesion to cement paste. Low-cost procedures and reagents were used in the surface treatment to minimize the final cost of the modified material. Among the surface treatments tested to enhance the hydrophilicity of the rubber surface, a sodium hydroxide (NaOH) solution gave the best result. The particles were surface-treated with NaOH saturated aqueous solutions for 20 minutes before using them in concrete. Then, scanning electron microscopy (SEM) and measurements of water absorption, density, flexural strength, compressive strength, abrasion resistance, modulus of elasticity 29 and fracture energy were performed using test specimens (W/C, water-to cementitiouse materials ratio as 0.36) containing 10% of powdered rubber or rubber treated with 10% NaOH. The test results showed that the NaOH treatment enhances the adhesion of tire rubber particles to cement paste, and mechanical properties such as flexural strength and fracture energy were improved with the use of tire rubber particles as addition instead of substitution for aggregate. The reduction in the compressive strength (33%) was observed, which is lower than that reported in the literature. Lee et al. (1998) developed ‘‘tire-added latex concrete’’ to incorporate recycled tire rubber as a part of concrete. Crumb rubber from used tires was used in TALC (tire-added latex concrete) as a substitute for fine aggregates or styrene–butadiene rubber (SBR) latex while maintaining the same water cementitiouse materials ratio. TALC showed higher flexural and impact strengths than those of Portland cement, latex modified concrete and rubber added concrete. Pictures taken using the SEM seem to support that there was better bonding between crumb rubber and Portland cement paste due to latex. TALC showed potential as a viable construction material that is less brittle than other types of concrete. Biel and Lee (1996) reported that the type of cement noticeably affects the compressive strength of rubcrete. They used two types of cement, magnesium oxychloride cement and Portland cement, in making rubcrete. The percentage of fine aggregate substitution varied from 0 to 90% by weight. It was observed that 90% loss in compressive strength occurred for 30 both Portland cement rubber concrete (PCRC) and magnesium oxychloride cement rubber concrete (MOCRC) when aggregates (90% of fine aggregate and 25% of total aggregate) were replaced by untreated rubber. Magnesium oxychloride cement concrete exhibited approximately 2.5 times the compressive strength of PCC for both inclusions of rubber and without inclusion of rubber in the concrete. In terms of splitting tensile strength, PCC specimens made with 25% of rubber by total aggregate volume retained 20% of their splitting tensile strength after initial failure, whereas the magnesium oxychloride cement concrete specimens with the same rubber content retained 34% of their splitting tensile strength. They further noted that use of magnesium oxychloride cement may provide high strength and better bonding characteristics to rubber concrete, and rubber concrete made with magnesium oxychloride cement could possibly be used in structural applications if rubber content is limited to 17% of the total volume of the aggregate. 2.5.5 Shrinkage A limited amount of literature is available concerning the plastic shrinkage of concrete containing rubber particles. Preliminary results reported by Raghvan et al. (1998) suggested that incorporation of rubber shreds (two different shapes of rubber particles as constituents of mortar: (1) granules, about 2 mm in diameter and (2) shreds having two sizes which were, nominally, 5.5 mm to 1.2 mm and 10.8 mm to 1.8 mm (length diameter) to mortar help in reducing plastic shrinkage cracking in comparison to control 31 mortar. Raghvan et al. (1998) further reported that control specimens developed cracks having an average width of about 0.9 mm, while the average crack width for specimens with a mass fraction of 5% rubber shreds was about 0.4 to 0.6 mm. It was also reported that onset time of cracking was delayed by the addition of 5% rubber shreds. Mortar without rubber 566 R. Siddique, T.R. Naik/Waste Management 24 (2004) 563–569 shreds cracked within 30 minutes, while mortar with 15% fraction by mass cracked after 1 hour. It was further indicated that the higher the content of rubber shreds, the smaller the crack length and width, and the onset time of cracking was more delayed. 2.5.6 Toughness and Impact Resistance Tantala et al. (1996) investigated the toughness (toughness is also known as energy absorption capacity and is generally defined as the area under load deflection curve of a flexural specimen) of a control concrete mixture and rubcrete mixtures with 5% and 10% buff rubber by volume of coarse aggregate. They reported that toughness of both rubcrete mixtures was higher than the control concrete mixture. However, the toughness of rubcrete mixture with 10% buff rubber (2 to 6 mm) was lower than that of rubcrete with 5% buff rubber because of the decrease in compressive strength. Tantala et al. (1996) Based on their investigations on use of rubber shreds (having two sizes which were, nominally, 5.5 mm to 1.2 mm and 10.8 mm to 1.8 mm) and granular (about 2 mm in diameter) rubber in mortar, Raghvan et al. (1998) reported that mortar specimens with rubber 32 shreds were able to withstand additional load after peak load. The specimens were not separated into two pieces under the failure flexural load because of bridging of cracks by rubber shreds, but specimens made with granular rubber particles broke into two pieces at the failure load. This indicates that post-crack strength seemed to be enhanced when rubber shreds are used instead of granular rubber. Khatib and Bayomy (1999) reported that as the rubber content is increased, rubcrete specimens tend to fail gradually and failure mode shape of the test specimen is either a conical or columnar (conical failure is gradual, whereas columnar is more of shreds having two sizes which were, nominally, 5.5 mm to 1.2 mm and 10.8 mm to 1.8 mm (length diameter) sudden failure). At a rubber content of 60%, by total aggregate volume, the specimens exhibited elastic deformations, which the specimens retained after unloading. Eldin and Senouci (1993) demonstrated that the failure mode of specimens containing rubber particles was gradual as opposed to brittle. Biel and Lee (1996) reported that failure of concrete specimens with 30, 45, and 60% replacement of fine aggregate with rubber particles occurred as a gradual shear that resulted in a diagonal failure, whereas failure of plain (control) concrete specimens was explosive, leaving specimens in several pieces. Goulias and Ali (1997) found that the dynamic modulus of elasticity and rigidity decreased with an increase in the rubber content, indicating a less stiff and less brittle material. They further reported that dampening capacity 33 of concrete (a measure of the ability of the material to decrease the amplitude of free vibrations in its body) seemed to decrease with an increase in rubber content. However, Topcu and Avcular (1997) recommended the use of rubberized concrete in circumstances where vibration damping is required. Similar observations were also made by Fattuhi and Clark (1996), and Topcu and Avcular (1997) reported that the impact resistance of concrete increased when rubber aggregates were incorporated into the concrete mixtures. The increase in resistance was derived from the enhanced ability of the material to absorb energy. Eldin and Senouci (1993), and Topcu (1995) also reported similar results. Olivares et al. (2002) have reported that addition of crumb tire rubber volume fractions up to 5% in a cement matrix did not yield a significant variation of the concrete mechanical features, either maximum stress or elastic modulus. 2.5.7 Freezing and Thawing Resistance Savas et al. (1996) carried out investigations to study the rapid freezing and thawing (ASTM C 666, Procedure A) durability of rubber concrete. Various mixtures were made by incorporating 10, 15, 20, and 30% ground rubber by weight of cement used for the control mixture. Based on their studies, they concluded that: (1) Rubcrete mixtures with 10% and 15% ground rubber (2 to 6 mm in size) exhibited durability factors higher than 34 60% after 300 freezing and thawing cycles, but mixtures with 20% and 30% ground rubber by weight of cement could not meet the ASTM standards (durability factor), (2) Air-entrainment did not provide improvements in freezing and thawing durability for concrete mixtures with 10, 20 and 30% ground tire rubber, and (3) Increase in scaling (scaling gives an evaluation of the surface exposed to freezing and thawing cycles as measured by the loss of weight) increased with the increase in freezing and thawing cycles. Benazzouk and Queneudec (2002) studied the freeze–thaw durability of cement–rubber composites through the use of two types of rubber aggregates. The types of the aggregates were: compact rubber aggregate (CRA) and expanded rubber aggregates (ERA). Volume-ratio of the aggregates ranged from 9% to 40%. The results showed improvements in the durability of the composite containing 30% and 40% rubber by volume. Improvement in the durability of the composite containing ERA type aggregates is better than composite made with CRA aggregates. The finding is more distinct for ERA type. Paine et al. (2002) investigated the use of crumb rubber as an alternative to air-entrainment for providing freeze–thaw resisting concrete. Three sizes of crumb rubber, 0.5 to 1.5, 2–8 and 5 to 25 mm were used. Test results showed that there is potential for using crumb rubber as a freeze–thaw resisting agent in concrete. The R. Siddique, T.R. Naik / Waste Management 24 (2004) 563–569 567 crumb rubber concrete performed 35 significantly better under freeze–thaw conditions than plain concrete, and the performance of crumb rubber concrete in terms of scaling was similar to that of air-entrained concrete. Studies presented in this chapter deals with the behavior of concrete and asphalt mixes after adding additives through replacement in different procedures, this leads to study more about the physical characteristics of concrete mixes in a different proportions and help in setting the methodology for this thesis as well as make a comparable analysis with the outcome of this thesis. 36 CHAPTER THREE METHODOLOGY 37 CHAPTER THREE METHODOLOGY 3.1 Introduction This thesis aims at utilizing rubber waste tires as a constituent in Portland cement concrete mixes and its products as a partial replacement of natural and artificial aggregate components. 3.2 Work Procedure The following represents the methodology by which to study the effect of utilizing waste crumb tires in Portland cement concrete mixes were done. 3.2.1 Materials The materials used in this thesis were obtained from Mawasi concrete plant in Nablus city (Nablus industrial area near Beit-Eiba village). The original source of crushed coarse aggregate are Abu Shusheh Crusher Corporation and Daymoona (Naqap desert area) for fine aggregate (sand), and grinded tires (crumb) was obtained from ALLOCK and SONS LTD (UK). Though, large amounts of waste tires exist in the West Bank area, no industries exist yet for the availability waste tires crumbs. The basic ingredients of PCC and its products, which were used in this research work, are: 38 1- Normal Portland cement (Cement type 1). 2- Natural Coarse aggregate (sedimentary rock source). 3- Natural Fine aggregate (sand). 4- Water (fresh drinkable water). 5- Grinded tires (fine crumb tires). 3.2.2 Raw Material Tests The raw materials used in this research work were tested for the purpose of identification of basic physical characteristics using the following tests: - Sieve analysis. (ASTM C-136) - Specific gravity and water absorption. (ASTM C-127) - Abrasion (Lose Angles abrasion test). (ASTM C-88) - Amount of fines and injurious particles (Sand equivalent) (ASTM D-2419). Tests results of the raw materials used will be presented in the following chapter of this thesis. 3.2.3 Plain Portland Cement Concrete Mixes Standard Portland cement concrete mixes without crumb rubber were made with different grades and different water cement ratios. These mixes were 39 used as a reference standard comparison mixes. Such mixes reflect the local design mixes used by the ready mix plants. Table 3.1 shows the proportions of the raw materials used for each grade for one cubic meter of Portland cement concrete. Table 3.2 shows the mix ingredients for a batch of 0.01 cubic meters. Table (3.1): Concrete mix design by weight of mix ingredients (kg/m3 of PCC) B-450B-300 B-250B-200B-150Concrete Grade 590 590 590 650 650 Coarse aggregate (size1) 220 220 220 220 220 Coarse aggregate (size2) 440 440 440 425 425 Coarse aggregate size3) 590580 580520500Sand 470 290 260 220 200 Cement 180- 200 180- 200 180- 200 180- 200 180-200Water Source: Mawasi Palestine Company for Concrete (2006) Table (3.2): Mix ingredients (kg/0.01m3 of PCC) B-450B-300 B-250B-200B-150Concrete Grade 12.50 12.50 12.50 12.95 12.95 Coarse aggregate 5.5 5.8 5.8 5.2 5.0 Fine aggregate (sand) 4.7 2.9 2.6 2.2 2.0 Cement 2.0 1.8 1.9 1.95 1.9 Water 0.430.62 0.730.890.95W/C 40 3.2.4 Crumb Portland Cement Concrete Mixes Portland cement concrete mixes utilizing crumb waste tires by volumetric replacement of sand with different proportions of replacements, basically 25, 50, 75, and 100% replacements were made. Tables 3.3 through 3.7 show the replacement of fine aggregate (sand) in different proportions by the crumb waste tires volumetric. By dividing the weight of sand to be replaced by crumb waste tires by its specific gravity, the volume of sand was obtained; this volume is to be replaced by volume of crumb tire waste converted to weight using the following physical characteristics which was tested as a part of this thesis: • Dry Rodded Weight of Sand = 1.431 g/cm3 • Dry Rodded Weight of crumbed tires waste = 0.640 g/cm3 • Specific Gravity of Sand = 2.644 g/cm3 • Specific Gravity of crumbed waste tires = 1.140 g/cm3 41 Table (3.3): Grade B-150 of PCC for batch mix B-150 0.0% of sand by weight is to be replaced by shredded tires Weight of sand (gm) Volume of sand (cm3) Equivalent Weight of shredded tires (Kg) 5000 1893.9 0.0 25% of sand by weight is to be replaced by shredded tires Weight of sand (gm) Volume of sand (cm3) Equivalent Weight of shredded tires (Kg) 1250 473.5 0.540 50% of sand by weight is to be replaced by shredded tires Weight of sand (gm) Volume of sand (cm3) Equivalent Weight of shredded tires (Kg) 2500 947.0 1.080 75% of sand by weight is to be replaced by shredded tires Weight of sand (gm) Volume of sand (cm3) Equivalent Weight of shredded tires (Kg) 3750 1420.5 1.619 100% of sand by weight is to be replaced by shredded tires Weight of sand (gm) Volume of sand (cm3) Equivalent Weight of shredded tires (Kg) 5000 1893.9 2.159 Table (3.4): Grade B-200 of PCC for batch mix B-200 0.0% of sand by weight is to be replaced by shredded tires Weight of sand (gm) Volume of sand (cm3) Equivalent Weight of shredded tires (Kg) 5200 1969.7 0.0 25% of sand by weight is to be replaced by shredded tires Weight of sand (gm) Volume of sand (cm3) Equivalent Weight of shredded tires (Kg) 1300 492.4 0.561 50% of sand by weight is to be replaced by shredded tires Weight of sand (gm) Volume of sand (cm3) Equivalent Weight of shredded tires (Kg) 2600 984.8 1.123 75% of sand by weight is to be replaced by shredded tires Weight of sand (gm) Volume of sand (cm3) Equivalent Weight of shredded tires (Kg) 3900 1477.3 1.684 100% of sand by weight is to be replaced by shredded tires Weight of sand (gm) Volume of sand (cm3) Equivalent Weight of shredded tires (Kg) 5200 1969.7 2.245 42 Table (3.5): Grade B-250 of PCC for batch mix B-250 0.0% of sand by weight is to be replaced by shredded tires Weight of sand (gm) Volume of sand (cm3) Equivalent Weight of shredded tires (Kg) 5800 2197.0 0.0 25% of sand by weight is to be replaced by shredded tires Weight of sand (gm) Volume of sand (cm3) Equivalent Weight of shredded tires (Kg) 1450 549.2 0.626 50% of sand by weight is to be replaced by shredded tires Weight of sand (gm) Volume of sand (cm3) Equivalent Weight of shredded tires (Kg) 2900 1098.5 1.252 75% of sand by weight is to be replaced by shredded tires Weight of sand (gm) Volume of sand (cm3) Equivalent Weight of shredded tires (Kg) 4350 1647.7 1.878 100% of sand by weight is to be replaced by shredded tires Weight of sand (gm) Volume of sand (cm3) Equivalent Weight of shredded tires (Kg) 5800 2197.0 2.505 Table (3.6): Grade B-300 of PCC for batch mix B-300 0.0% of sand by weight is to be replaced by shredded tires Weight of sand (gm) Volume of sand (cm3) Equivalent Weight of shredded tires (Kg) 5800 2197.0 0.0 25% of sand by weight is to be replaced by shredded tires Weight of sand (gm) Volume of sand (cm3) Equivalent Weight of shredded tires (Kg) 1450 549.2 0.626 50% of sand by weight is to be replaced by shredded tires Weight of sand (gm) Volume of sand (cm3) Equivalent Weight of shredded tires (Kg) 2900 1098.5 1.252 75% of sand by weight is to be replaced by shredded tires Weight of sand (gm) Volume of sand (cm3) Equivalent Weight of shredded tires (Kg) 4350 1647.7 1.878 100% of sand by weight is to be replaced by shredded tires Weight of sand (gm) Volume of sand (cm3) Equivalent Weight of shredded tires (Kg) 5800 2197.0 2.505 43 Table (3.7): Grade B-450 of PCC for batch mix B-450 0.0% of sand by weight is to be replaced by shredded tires Weight of sand (gm) Volume of sand (cm3) Equivalent Weight of shredded tires (Kg) 5900 2234.8 0.0 25% of sand by weight is to be replaced by shredded tires Weight of sand (gm) Volume of sand (cm3) Equivalent Weight of shredded tires (Kg) 1475 558.7 0.637 50% of sand by weight is to be replaced by shredded tires Weight of sand (gm) Volume of sand (cm3) Equivalent Weight of shredded tires (Kg) 2950 1117.4 1.274 75% of sand by weight is to be replaced by shredded tires Weight of sand (gm) Volume of sand (cm3) Equivalent Weight of shredded tires (Kg) 4425 1676.1 1.911 100% of sand by weight is to be replaced by shredded tires Weight of sand (gm) Volume of sand (cm3) Equivalent Weight of shredded tires (Kg) 5900 2234.8 2.548 3.3 Tests on PCC Slump test was made on fresh concrete to measure the effect of change in ingredients on workability according to the addition of crumb waste tires. The following tests on hardened concrete were made using four specimens (cubes) from each proportion made: - Compressive Strength (PS-55): It is worth to note that the Palestinian standard requires a 7 days curing while the ASTM standards require a curing conditions 28 days curing after casting the molds. - Water Absorption (ASTM C-642). 44 - Abrasion (ASTM C-944). - Modulus of Elasticity (ASTM C-469). - Weight before replacement and weight after replacement. 3.4 Thermal and Sound Insulation testing For sound and thermal insulation, a concrete wood mold having a dimension of 15x15x5cm was made, three specimens of each proportion were made as shown in Figure 3.1 with 0.0%, 25%, 50%, 75% and 100% crumbed waste tires with properties same as that of concrete cubes mixes. Figure 3.1: Concrete mold (15x15x5cm Dimension) 45 A wooden box was made in a way that the heat will be directly move or transfer from one chamber having constant temperature exposed on one of the faces of the specimen for a period of time through the specimen to another chamber. The temperature was measured until the temperature became constant in the two faces of concrete specimen using a laser thermometer (High Temperature Infrared Thermometer, Type K/J/T/E/R). Figures 3.2, 3.3, and 3.4 show the mechanism of the testing. Figure 3.2: Wooden box face with two opening one for source and the other for measuring (40x40x100cm Dimension) 46 Figure 3.3: Wooden box back (the other face) with one opening for measuring. Figure 3.4: Specimen location (at the middle of the wooden box) with frame dimension 15x15x15 cm 47 The same procedure was made for testing the sound insulation using a constant noise source and a noise measuring device (Sound Level Meter Auto range, RS – 232). 48 CHAPTER FOUR EXPERIMENTAL TESTS RESULTS 49 CHAPTER FOUR EXPERIMENTAL TESTS RESULTS 4.1 Introduction This chapter presents a summary of the results which were obtained from laboratory tests that have been done on the samples. Tests were done on materials (fine and coarse aggregates), fresh and hardened concrete. 4.2 Materials Testing Results Table 4.1 summarizes the tests results of the properties of materials used in this thesis. Notice that these materials are used locally in West Bank by concrete plants, and Figure 4.1 gives the specification of aggregates used in the mixes. 50 Table (4.1): Materials tests results RESULTS OF AGGREGATE TESTING 1- Gradation (ASTM C-136) Sieve No. 1" 3/4" 1/2" 3/8" # 4 # 8 # 16 # 30 # 50 # 100 # 200 Coarse aggregate Pe rc en t Pa ss in g 100 75 59 54 26 11 3.9 3.3 2.8 2.5 2.4 Fine aggregate - - 100 100 99.0 97.0 92.2 64.6 26.3 6.1 3.9 Crumb tires - - - - - - - 100 47.4 26.7 0.0 No. Type of test Standard Unit Result Coarse aggregate Fine aggregate Shredded tires 2. Bulk specific gravity ASTM C-127 - 2.560 2.521 1.131 3. Specific gravity (Saturated surface Dry – SSD) - 2.621 2.640 1.140 4. Specific gravity. (Apparent) - 2.716 2.734 1.152 5. Water absorption % 1.02 0.5 - 6. Los Angeles abrasion ASTM C-88 % 30.1 - - 7. Sand equivalent ASTM D-2419 - - 66.0 - 8. Clay lumps and friable particles ASTM-C142 % 1.1 - - 51 Figure 4.1: Particle size distribution 0 10 20 30 40 50 60 70 80 90 1000.01 0.1 1 10 100 Sieve size (m m ) P ercen t P a ssin g (% ) crumb waste tires fine agregate (sand) Coarse aggregate 52 4.3 Concrete Compressive Strength and Slump Tests Results Table 4.2 summarizes concrete compressive strength and slump tests results for different types of concrete with and without replacement of sand. Table (4.2): Concrete compressive strength test results Concrete Grade Percent replacement (%) Average compressive strength at 28 days (kg/cm2) Slump (mm) B-150 0.0 159.1 23.0 25 117.0 24.0 50 92.4 23.0 75 69.8 25.0 100 53.6 24.0 B-200 0.0 178.2 26.0 25 154.9 25.0 50 111.4 27.0 75 77.9 26.0 100 60.9 28.0 B-250 0.0 290.1 25.0 25 238.1 30.0 50 152.5 28.0 75 102.3 26.0 100 74.4 27.0 B-300 0.0 313.5 29.0 25 235.1 30.0 50 156.0 28.0 75 98.5 26.0 100 67.1 29.0 B-450 0.0 472.6 25.0 25 284.8 30.0 50 227.7 29.0 75 144.6 26.0 100 92.6 25.0 53 4.4 Density Test Results Table 4.3 summarizes densities for different categories of PCC with and without replacement. Table (4.3): Density test results Concrete Grade Percent replacement (%) Density (Kg/m3) B-150 0.0 2336.0 25 2196.0 50 2153.0 75 2065.0 100 1961.0 B-200 0.0 2378.0 25 2214.0 50 2174.0 75 2078.0 100 2002.0 B-250 0.0 2406.0 25 2258.0 50 2148.0 75 2089.0 100 1949.0 B-300 0.0 2395.0 25 2259.0 50 2095.0 75 2083.0 100 1941.0 B-450 0.0 2430.0 25 2190.0 50 2155.0 75 2028.0 100 1949.0 54 4.5 Water Absorption Test Results Table 4.4 summarizes concrete water absorption test results for different types of concrete with and without replacement of sand. Table (4.4): Concrete water absorption test results Concrete grade Percent replacement by crumb tires Saturated surface dry weight Oven dry weight Water absorption - (%) (gm) (gm) (%) B-150 0.0 2555.0 2414.4 5.8 25.0 2304.0 2188.7 5.3 50.0 2323.0 2193.5 5.9 75.0 2192.0 2060.6 6.4 100 2094.0 1955.8 7.1 B-200 0.0 2664.0 2519.4 5.7 25.0 2420.0 2294.4 5.5 50.0 2395.0 2263.7 5.8 75.0 2203.0 2074.4 6.2 100 2124.0 1986.5 6.9 B-250 0.0 2534.0 2392.0 5.9 25.0 2415.0 2295.5 5.2 50.0 2260.0 2134.4 5.9 75.0 2230.0 2101.5 6.1 100.0 2073.0 1940.7 6.8 B-300 0.0 2484.0 2347.2 5.8 25.0 2481.0 2349.2 5.6 50.0 2359.0 2230.2 5.8 75.0 2282.0 2152.5 6.0 100.0 2071.0 1941.4 6.7 B-450 0.0 2629.0 2485.1 5.8 25.0 2462.0 2334.4 5.5 50.0 2412.0 2275.1 6.0 75.0 2241.0 2100.1 6.7 100.0 2012.0 1861.4 8.1 55 4.6 Abrasion Test Results Table 4.5 summarizes Abrasion test results. Table (4.5): Concrete abrasion test results Concrete Grade Percent replacement (%) Average loss (gm) B-150 0.0 3.0 25 3.4 50 4.2 75 4.9 100 5.4 B-200 0.0 2.6 25 2.7 50 3.0 75 4.1 100 4.5 B-250 0.0 2.5 25 5.7 50 7.6 75 7.7 100 10.3 B-300 0.0 2.0 25 6.6 50 6.9 75 7.2 100 9.6 B-450 0.0 1.4 25 3.2 50 3.8 75 6.3 100 7.4 56 4.7 Modulus of Elasticity Test Results (E) Table 4.6 summarizes modulus of elasticity test results for various PCC categories. Table (4.6): Modulus of elasticity test results Concrete Grade Percent replacement (%) Modulus of elasticity E (KN/mm) B-150 0.0 131.3 25 100.5 50 76.2 75 45.5 100 24.1 B-200 0.0 143.2 25 113.4 50 94.6 75 60.5 100 34.2 B-250 0.0 232.0 25 186.1 50 122.4 75 75.9 100 48.5 B-300 0.0 234.2 25 196.3 50 126.3 75 86.1 100 53.9 B-450 0.0 379.2 25 231.6 50 177.6 75 120.3 100 74.6 57 4.8 Noise Insulation Test Results Table 4.7 consists of test results of noise insulation in percent reduction of noise as an expression of noise insulation at low and high noise levels for various PCC categories. Table (4.7): Noise insulation test results Concrete Grade Percent replacement (%) Percent reduction (Low) (%) Percent reduction (High) (%) B-150 0.0 14.6 13.7 25 15.1 13.9 50 16.3 14.6 75 17.4 15.1 100 18.8 17.7 B-200 0.0 14.1 13.5 25 15.3 14.1 50 16.5 14.7 75 17.6 16.4 100 18.6 17.2 B-250 0.0 13.9 13.5 25 15.4 13.8 50 16.7 14.4 75 17.9 15.5 100 18.3 17.8 B-300 0.0 14.4 13.3 25 15.0 13.9 50 16.1 14.3 75 16.8 14.9 100 17.9 17.1 B-450 0.0 14.3 13.6 25 14.9 14.2 50 15.8 15.1 75 17.1 16.6 100 18.2 18.1 58 4.9 Thermal Insulation Test Results Table 4.8 consists of test results of thermal insulation in percent reduction of temperature as an expression of thermal insulation at a constant source of heat for various PCC categories. Table (4.8): Thermal insulation test results Concrete Grade Percent replacement (%) Percent reduction Of temperature (%) B-150 0.0 24.3 25 25.1 50 27.8 75 30.5 100 32.6 B-200 0.0 24.5 25 25.2 50 28.0 75 30.7 100 32.8 B-250 0.0 22.9 25 23.6 50 25.5 75 27.8 100 29.6 B-300 0.0 23.3 25 23.8 50 26.1 75 28.6 100 30.1 B-450 0.0 22.7 25 24.3 50 26.2 75 27.5 100 29.3 59 CHAPTER FIVE ANALYSIS OF RESULTS 60 CHAPTER FIVE ANALYSIS OF RESULTS 5.1 Introduction This chapter aims at analyzing the tests results to show how concrete behavior will change as a result of the volumetric replacement of sand with crumb waste tires when compared to standard mixes of PCC containing no crumb waste tires. 5.2 Compressive Strength In the analysis of the laboratory results for compressive strength, Figure 5.1 gives the basic relationship of the percentage of replacement by crumb waste tires with the compressive strength for concrete category of B-150. Figure 5.1: Percent replacement by crumb waste tires versus compressive strength for PCC-150 0 20 40 60 80 100 120 140 160 180 0 20 40 60 80 100 Percent replacement C om pr es si ve st re ng th k g/ cm 2 61 As a result of a volumetric replacement of sand by crumb waste tires, compressive strength decreases as percent of crumb waste tires increases as shown in Figure 5.1, at zero replacement, compressive strength is 159.0 kg/cm2, while at 25% replacement the compressive strength decreases to 117.0 kg/cm2 that is a decrease of 26.4%. At 50% replacement, compressive strength is 92.4 kg/cm2 that is a decrease of 41.9% from the original value. For the replacements of 75 and 100% replacement, the compressive strength drops to 56 and 66.3% respectively from the original reference value. Figure 5.2 shows compressive strength for concrete grade B-150 and B-200 versus percent replacement by crumb waste tires. For concrete grade of B- 200 the compressive strength is 178.2, 154.9, 111.4, 77.9, 60.9 kg/cm2 for replacement values of 0, 25, 50, 75, and 100% respectively. The percentage drop reflecting those percentages is 13, 37.5, 56.3, and 65.8% respectively. In comparison between the concrete grades of B-150 and B-200, it can be noticed that differences are 24.5, 17.1, 10.4, and 12% for 25, 50, 75, and 100% replacements respectively. This implies that as the percentage replacement increases, the percentage difference between the two categories decreases with higher overall drop in compressive strength for concrete category for B-250. 62 Figure 5.2: Percent replacement by crumb waste tires versus compressive strength for PCC-150+200 0 50 100 150 200 0 20 40 60 80 100 120 Percent replacement C om pr es siv e st re ng th k g/ cm 2 B-150 B-200 Figure 5.3 shows the compressive strength for concrete grades B-150, B- 200, B-250, B-300, and B-450 versus percent replacement by crumb waste tires. For concrete grade B-250 with zero replacement the compressive strength is 290.0 kg/cm2. At 25% replacement the compressive strength is 238.1 kg/cm2 that is a decreases of 17.9% from the original value, while for 50, 75, and 100% replacement the compressive strength decreases to 47.4, 64.7, and 74.3% respectively. Comparing B-150 and B-250, B-150 as a reference, for a 25% replacement the compressive strength decreases to 50.9%, while for 50, 75, and 100% replacements, the compressive strength decreases to 39.4, 31.7, and 28% from those of concrete B-250 grade. For PCC B-300 the compressive strengths are 313.5, 235.1, 156.0, 98.5, 67.1 kg/cm2 for 0, 25, 50, 75 and 100% replacement respectively, giving 63 decreases in compressive strength of 25, 50, 68.6, and 78.6% respectively from the original value. When comparing B-250 with B-300 it is noticed that at 25, 50, 75, and 100% replacements the difference is 1.3, 2.3, 3.7, and 9.8% respectively. It is also noticed that concrete grade B-250 is slightly better for compressive strength compared to B-300. For B-450 the compressive strength is 472.6, 284.8, 227.7, 144.6, 92.6 kg/cm2 for replacements values of 0, 25, 50, 75, and 100% respectively. The percentage drop reflecting those percentages is 39.7, 51.8, 69.4, and 80.4% respectively. In comparing B-300 with B-450, it is noticed that at 25, 50, 75, and 100% the differences are 21, 46, 46.8, and 38.0% respectively. Figure 5.3: Percent replacement by crumb waste tires versus compressive strength for various PCC categories 0 100 200 300 400 500 0 20 40 60 80 100 Percent replacement C om pr es siv e st re ng th k g/ cm 2 B-150 B-200 B-250 B-300 B-450 Figure 5.4 shows also how compressive strength changed with percent of volumetric replacement of sand by waste crumb tires relative to the specified compressive strength. 64 Notice actual compressive strength at 0, 25, 50, 75, and 100% replacement for grades B-150, 200, 250, 300, and B-450, actual compressive strength differences are less decreased at concrete grades B-150 and B-200 versus replacement, differences of compressive strength increases at concrete grades B-250, 300, and B-450 versus replacement. As an example; for concrete grade of B-450 the differences between compressive strengths are 39.7, 20.0, 36.5, and 36.0%, while for concrete grade of B-200 the differences are 13.1, 28.1, 30.1, and 21.8%. Figure 5.4: Compressive strength of Portland cement concrete for various percentages of replacements of crumbed waste tires 0 50 100 150 200 250 300 350 400 450 500 150 200 250 300 350 400 450 Specified compressive strength (kg/cm2) A ct ua l co m pr es si ve st re ng th (k g/ cm 2) 0% Replacement 25% Replacement 50% Replacement 75% Replacement 100% Replacement Figure 5.4 shows how actual compressive strength decreased at specified compressive strength with increasing percent of replacement of waste crumb tires. This happened because as replacement increases, bonding between aggregate particles and cement decrease, and because of the weakness of waste crumb rubber particles with comparison to sand. 65 5.3 Density Density of concrete also decreases as crumb waste tires increases, see Figure 5.5 which presents how density decreases when crumb waste tires increases for PCC-150. Densities are 2330, 2196, 2153, 2065, and 1961 kg/m3 for replacement of 0, 25, 50, 75, and 100% respectively. Those replacement shows decrease of density in which the density decreases to 5.8, 7.6, 11.4, and 15.8% with reference to zero replacement. Figure 5.5: Perecent replacement by crumb waste tire versus density for PCC-150 1900 2000 2100 2200 2300 2400 0 20 40 60 80 100 Percent replacement D en si ty k g/ m 3 Note that the difference of densities for various PCC versus replacement in Figure 5.6. In addition, Notice the difference between B-150 and B-200, at 0, 25, 50, 75, and 100% replacement are 1.8, 0.8, 0.9, 0.6, and 2.1% respectively. 66 For B-200 and B-250, the differences are 1.2, 2, 1.2, 0.5, and 2.6%. For B- 250 and B300 comparison differences are 0.5, 0.04, 2.5, 0.3, and 0.4%. Finally for B-300 with comparison by B-450 differences are 1.5, 3.1, 2.9, 2.6, and 0.4%. Theses differences show slight differences in densities between different PCC categories versus replacement, but the decreases for each type on density reaches between (16-19%) at 100% replacement. Figure 5.6: Perecent replacement by crumb waste tire versus density for various categories of concrete 1900 2000 2100 2200 2300 2400 2500 0 20 40 60 80 100 Percent replacement D en sit y kg /m 3 PCC 150 PCC 200 PCC 250 PCC 300 PCC 450 Generally, density decreases as percent replacement increases since waste crumb rubber has less specific gravity than sand. 67 5.4 Water Absorption To analyze tests results of water absorption see Figure 5.7 that shows the basic relation between water absorption versus percent replacement of waste crumb tires for PCC-150. Notice how water absorption behaves as replacement increase at 0, 25, 50, 75, and 100. Figure 5.7: Perecent replacement by crumb waste tire versus Water Absorption for PCC-150 5 6 7 8 0 20 40 60 80 100 Percent replacement W at er A bs or pt io n (% ) Water absorption decreases at 25% replacement and pounces back approximately to its original value at 50% replacement and starts to increase as waste crumb tires increases (see Figure 5.7 for PCC-150). Figure 5.8 shows the differences between water absorption for different PCC categories versus replacement. For B-150 and B-200 the differences are 1.7, 3.6, 1.7, 3.1, and 2.8% for 0, 25, 50, 75, and 100% replacements respectively. 68 For B-200 and B-250 differences are 3.3, 5.5, 1.7, 1.6, and 1.4% for 0, 25, 50, 75, and 100% replacements respectively. For B-250 and B-300 differences are 1.7, 7.1, 1.7, 1.6, and 1.5 for 0, 25, 50, 75, and 100% replacement respectively. For B-300 and B-450 differences are 0.0, 1.8, 3.3, 10.4, and 17.3 for 0, 25, 50, 75, and 100% replacement respectively. Figure 5.8: Perecent replacement by crumb waste tire versus Water Absorption for various categories of concrete 5 6 7 8 9 0 20 40 60 80 100 Percent replacement W at er A bs or pt io n (% ) PCC 150 PCC 200 PCC 250 PCC 300 PCC 450 This leads to the idea that water absorption decreased at 25% replacement since voids are decreased but occasional vacuums existed when waste crumb tires replacement increased which causes an increase in water absorption. In addition, weakness of bonding between particles will increase absorption which permits water to enter through voids in the interface between the crumbs and the cement paste as a result of increasing waste crumb tires. It is worth to note that the waste crumb tires have smaller particle size compared to that of sand as seen in Figure 4.1. 69 5.5 Slump (Consistency) Slump is an expression of consistency, as slump increases the concrete blend is more consistent. Figure 5.9 shows slump versus replacement for different PCC categories. Figure 5.9: Percent replacement by crumb waste tires versus slump for various PCC categories 10 15 20 25 30 35 0 20 40 60 80 100 Percent replacement Sl um p (m m ) B-150 B-200 B-250 B-300 B-450 Slump showed little change in consistency during all mixing; slump ranges from 20-30 mm, there was no effect of increasing waste crumb tires replacement on consistency. This is because of the coarseness of the mixes and the existence of high adhesion forces between waste crumb particles and aggregate particles which prevents mixes to be more consistent. 5.6 Abrasion Figure 5.10 represents abrasion test results for concrete versus percent replacement for PCC-150. 70 Figure 5.10: Percent replacement by crumb waste tires versus abrasion for PCC-150 2 2.5 3 3.5 4 4.5 5 5.5 6 0 20 40 60 80 100 Percent replacement A br as io n (g m ) It is noticed that abrasion increases when replacement increases for grade B-150, this is because of the increase of waste crumb tires replacement. This happened because of the existing of fine crumb waste tires which has a weak resistance and of the weakness of bonding between the blend particles due to increasing of waste crumb tires percent replacement. On the other hand sand has a coarse surface texture and because of the nature micro structures of sand (silica quarts) that made bonding stronger with comparison to rubber. For 0, 25, 50, 75, and 100% replacement, the average loss by weight was increasing 13.3, 40, 63.3, and 80% respectively from the zero replacement. Figure 5.11 shows abrasion resistance versus replacement for different PCC categories. 71 Figure 5.11: Percent replacement by crumb waste tires versus abrasion for various PCC categories 0 2 4 6 8 10 12 0 20 40 60 80 100 Percent replacement A br as io n (g m ) B-150 B-200 B-250 B-300 B-450 Figure 5.11 shows obviously that abrasion increases as waste crumb tires increase because of the reasons mentioned above. 5.7 Modulus of Elasticity The modulus of elasticity is a measure of the stiffness of a material, or in this case it is a measure of the deformation of the rubberized concrete. Figure 5.12 shows stress versus strain relation. Figure 5.12: Stress versus strain for PCC-300 0 50 100 150 200 250 300 0 1 2 3 4 5 6 7 8Strain (mm) St re ss K N 25% 50% 75% 100% 0.0% 72 From the above Figure modulus of elasticity can be calculated by finding the slope which presents stress divided by strain for the first half of the curve, notice how the mode of failure changes when replacement of waste crumb tires increases. This means that the lower the modulus of elasticity of the sample, the lower the amount of deformation it could withstand before breaking. Figure 5.13 shows modulus of elasticity versus replacement of waste crumb tires for different categories of PCC. Modulus of elasticity decreased as waste crumb tires replacement increased. Figure 5.13: Percent replacement by crumb waste tires versus elasticity for various PCC 0 50 100 150 200 250 300 350 400 0 20 40 60 80 100 Percent replacement E la st ic ity (K N /m m ) B-150 B-200 B-250 B-300 B-450 5.8 Noise Insulation Figure 5.14 shows results of noise insulation at low level of noise (86.5 dp), this Figure presents percent replacement of waste crumb tires versus percent reduction of noise at low level for various PCC categories. 73 Figure 5.14: Percent replacement of waste crumb tires versus reduction of noise at low level for various PCC categories 13 14 15 16 17 18 19 0 20 40 60 80 100 Replacement % R ed uc tio n 150 low 200 low 250 low 300 low 450 low Average Low Figure 5.14 shows obviously the behavior of noise, as replacement increased, higher reduction of noise, this means that when replacement increased insulation increased. From the above Figure the reduction increased from 14% at 0% replacement to approximately 19% at 100% replacement. Figure 5.15 also presents percent replacement of waste crumb tires versus percent reduction of noise at high noise level (98.6 dp) for various PCC categories. 74 Figure 5.15: Percent replacement of waste crumb tires versus noise reduction at high level for various PCC categories 13 14 15 16 17 18 19 0 20 40 60 80 100 Replacement % R ed uc tio n 150 high 200 high 250 high 300 high 450 high Average High The above Figure shows the same behavior as low noise level but with less noise reduction or less insulation. Reduction of noise increased from 13.5% approximately at 0.0% replacement to 18% at 100% replacement. Figure 5.16 shows percent replacement versus averages of noise reduction at low and high levels. 75 Figure 5.16: Percent replacement of waste crumb tires versus average reduction of noise at low and high level 13 14 15 16 17 18 19 0 20 40 60 80 100 Replacement % R ed uc tio n Average High Average Low At low noise level higher insulation of noise occurred than high level of noise which easily noticed from Figure 5.16. The difference between reduction of noise at low level and high level, at 0, 25, 50, 75, and 100% is 0.74, 1.16, 1.66, 1.66, and 0.78 respectively, that gives higher increasing at low level of 5.5, 8.3, 11.4, 10.6, and 4.4% than the high noise level with an overall average of 8.0%. The more the material is brittle it will have lower noise insulation; the more the material is elastic it will have higher noise insulation. This means that when percent replacement increased concrete absorption of noise increased. Concrete with different percent replacement can isolate noise at low level better than high noise level, since concrete can absorb vibration at low level better than high level. 76 5.9 Thermal Insulation Figure 5.17 shows results of thermal insulation at a constant source of heat (54 C°), this Figure presents percent replacement of waste crumb tires versus percent reduction of temperature for various PCC categories. Figure 5.17 shows that percent reduction in temperature increased as waste crumb tires replacement increased, that leads the fact that thermal insulation increased as the percent replacement increased. No significant changes can be noticed between various PCC categories. Figure 5.17: Percent replacement of waste crumb tires versus temperature reduction for various PCC categories 22 24 26 28 30 32 34 0 20 40 60 80 100 Replacement % R ed uc tio n 150 200 250 300 450 Average Figure 5.18 shows the average percent reduction of temperature versus percent replacement of waste crumb tires for all PCC categories. Average reduction increased as percent replacement increased, at 0, 25, 50, 75, and 100% replacement percent reduction is 23.5, 24.4, 26.7, 29.0, and 77 30.9% respectively, which means that thermal insulation increased 3.8, 13.6, 23.4, and 31.5% from zero percent replacement. Figure 5.18: Percent replacement of waste crumb tires versus average temperature reduction for various PCC categories 22 24 26 28 30 32 34 0 20 40 60 80 100 Replacement % R ed uc tio n Average This behavior happened because when the material density is lowered thermal insulation increased, and because of lower conductivity that rubber has with comparison of concrete. 5.10 Particles Distributions Particles were distributed homogeneously in all mixes for 0, 25, 50, 75, and 100% replacement. In 25% replacement concrete blending was dense. It can be noticed that concrete blending is denser in 75% and 100% replacement, but still with homogeneous distribution of the particles through all percent replacement of mixes (See Figure 5.19). 78 Figure 5.19: Particles distribution (0, 25, 50, 75, and 100 % replacement from right to left) 79 CHAPTER SIX CONCLUSIONS AND RECOMMENDATIONS 80 CHAPTER SIX CONCLUSIONS AND RECOMMENDATIONS 6.1 Introduction This thesis aims to investigate the behavior of PCC mixes and the effect of utilizing waste crumb tires in these mixes. 6.2 Conclusions Based on the results and analysis done as a part of this research thesis, the following can be concluded: 1. Compressive strength decreases as the percent of waste crumb tire replacement increases for various PCC categories. 2. Density decreases as the percent of waste crumb tire replacement increases for various PCC categories. 3. Water absorption decreases at 25% replacement and pounces back approximately to its original value at 50% replacement, and then starts to increase as waste crumb tires increases. 4. Slump test results showed no change in consistency during all mixes; there was no effect of increasing waste crumb tires replacement on consistency. 81 5. Abrasion increases as waste crumb tires increases. 6. Modulus of elasticity decreases as waste crumb tires replacement increases. 7. Noise insulation increases as percent of crumb waste tires increases. At low noise levels, higher insulation of noise occurred than that of high levels of noise. 8. Thermal insulation increases as waste crumb tires percent increases. 6.3 Recommendations Based on the conclusions drawn above and the laboratory observations, the following are recommended: 1. Since the addition of crumb tires decreases compressive strength, it is recommended to use waste crumb tires for non structural Portland cement concrete in buildings such as floor slabs, floor ribs, under ground slabs, behind building stones and in partitions etc. 2. It is recommended to use percent of replacements in the vicinity of 25% in the PCC, since compressive strength still within the acceptable range, also good thermal and noise insulation can be achieved. 82 3. It is recommended to use replacements in an increment of 10% for better identification behavioral changes in the physical characteristics in future research. 4. It is recommended to study the effect of larger sizes of shredded tires on PCC. 5. It is recommended to further test the physical characteristics of PCC through shrinkage limit, permeability etc. 6. It is recommended to explore the effect of other raw materials in these mixes and study the changes in physical characteristics. 7. 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Waste Management, 26, pp 1033-1044. 90 APPENDICES 91 APPENDIX A COMPRESSIVE STRENGTH TEST RESULTS TABLES 92 Table 1: CONCRETE COMPRESSIVE STRENGTH TEST RESULTS (B-150) Sample Type Cubes 10x10x10 cm Place of Curing An - Najah Labs Standard Method PS-55 Concrete Type Standard mix with 0.0% volumetric replacement of sand No. Del. No. Weight Casting date Testing date Age Slump Crushing load Comp. strength تاريخ الصب الوزن االرسالية الرقم تاريخ مقاومة حمل الكسر التھدل العمر الفحص الضغط - - (g) - - (day) (mm) (KN) (Kg/cm2) 1 - 2329 5.12.06 6.1.07 32 20-30 152.0 155.0 2 2342 154.0 157.1 3 2338 162.0 165.2 Summaryملخص النتيجة يوماً 28المقاومة بعد معدل 28 day strength (kg/cm2) النسبة من المقاومة المطلوبة % of required strength 159.1 106% Table 2: CONCRETE COMPRESSIVE STRENGTH TEST RESULTS (B-150) Sample Type Cubes 10x10x10 cm Place of Curing An - Najah Labs Standard Method PS-55 Concrete Type Standard mix with 25% volumetric replacement of sand No. Del. No. Weight Casting date Testing date Age Slump Crushing load Comp. strength الصب تاريخ الوزن االرسالية الرقم تاريخ مقاومة حمل الكسر التھدل العمر الفحص الضغط - - (g) - - (day) (mm) (KN) (Kg/cm2) 1 - 2250 3.2.07 3.3.07 28 20-30 125.0 127.5 2 2173 104.0 106.1 3 2142 109.0 111.2 4 2219 120.6 123.0 Summaryملخص النتيجة يوماً 28المقاومة بعد معدل 28 day strength (kg/cm2) النسبة من المقاومة المطلوبة % of required strength 117.0 80% 93 Table 3: CONCRETE COMPRESSIVE STRENGTH TEST RESULTS (B-150) Sample Type Cubes 10x10x10 cm Place of Curing An - Najah Labs Standard Method PS-55 Concrete Type Standard mix with 50% volumetric replacement of sand No. Del. No. Weight Casting date Testing date Age Slump Crushing load Comp. strength تاريخ الصب الوزن االرسالية الرقم تاريخ مقاومة حمل الكسر التھدل العمر الفحص الضغط - - (g) - - (day) (mm) (KN) (Kg/cm2) 1 - 2195 3.2.07 3.3.07 28 20-30 90.7 92.5 2 2154 88.7 90.5 3 2125 92.4 94.2 4 2141 90.7 92.5 Summaryملخص النتيجة يوماً 28المقاومة بعد معدل 28 day strength (kg/cm2) النسبة من المقاومة المطلوبة % of required strengt